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Ii 10 Second Avenue South,#ED7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hItp.U_) ww.mecampbell,com E-mail main@mccampbell coin <br /> I <br /> Advanced GeoEnvrromnental Chent Project lD Chase-Van Buren Date Sampled 11/04/98 <br /> 4005 North Wilson Way <br /> Date Received 11/06/98 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 11/09-11/10/98 <br /> Client P O Date Analyzed 11109-11/10/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 98254 <br /> Client ID MW-6/11-4-98 <br /> Matnx W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<10 Ethylbcnzene 150 <br /> Benzene 91 Hexachlorobutadiene ND<5 <br /> Bromobenzene ND<5 lodomethane ND<5 <br /> Bromochloromethane ND<5 lsopropylbenzene 7 9 <br /> I Bromodichloromethane ND<5 p-Isopropyl toluene ND<5 <br /> Bromofonn ND<5 Methyl butyl ketone ND<5 <br /> Bromomethane ND<5 Methylene Chloride"' N11<5 <br /> n-Butyl benzene 20 Methyl ethyl ketone ND<5 <br /> sec-Butyl benzene ND<5 Methyl isobuty]ketone ND<5 <br /> tent-Butyl benzene ND<5 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<5 Napthalene 42 <br /> Carbon Tetrachloride ND<5 n-Propyl benzene ND<5 <br /> Chlorobenzene ND<5 Styrene W ND<5 <br /> Chloroethane ND<5 1,1,1,2-Tetrachloroethane ND<5 <br /> 2-Chloroethyl Vinyl Ether` NDS 1,1,2,2-Tetrachloroethane ND<5 <br /> Chloroform ND<5 Tetrachloroethene ND<5 <br /> Chloromethane ND<5 Toluene ND<5 <br /> 2-Chlorotoluene ND<5 1,2,3-Tnchlorobenzene ND<5 <br /> 4-Chlorotolucne ND<5 1,2,4-Tnchlorobenzene ND<5 <br />' Dibromochloromethane ND<5 1,I,1-Trichloroethane ND<5 <br /> 1,2-Dibromo-3-ch]oropropane ND<5 1,1,2-Tnchloroethane ND<5 <br /> Dibromomethane ND<5 Trichloroethene ND<5 <br /> 1,2-Dichlorobenzene ND<5 Tnehlorofluoromethane ND<5 <br /> 1,3-Dichlorobenzene ND<5 1,2,3-Tnchloropropane ND<5 <br /> 1,4-Dichlorobenzene ND<5 1,2,4-Tnmethylbenzene 150 <br /> Dichlorodifluoromethane ND<5 1,3,5-Tnmethylbenzene 23 <br /> 1,1-Dichloroethane ND<5 Vinyl Acetate"I ND<5 <br /> 1,2-Dichloroethane ND<5 Vinyl Chloride'" ND<5 <br /> 1,1-Dichloroethene ND<5 Xylenes,total `° 160 <br /> cis-1,2-Dichloroethene ND<5 <br /> trans-l,2-Dichloroethene ND<5 <br />' 1,2-Dichloropropane ND<5 <br /> 1,3-Dichloropropane ND<5 <br /> 22-Dichloropropane ND<5 Comments <br /> I,1-Dichloropropene ND<5 Surrogate Recoi cries(%) <br />' cis-1,3-Dichloropropene ND<5 Dibromofluoromethane 99 <br /> trans-l,3-Dichloropropene ND<5 Toluene-d8 99 <br /> Ethylene dibromide ND<5 4-Bromofluorobenzene 105 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts m ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (r) liquid sample that contains greater than ,5 vol % <br /> sediment,0)sample diluted due to high organic content, (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,0)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 /451—Edward Hartulton, Lab Director <br />