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MATRIX SPIRE SAMPLE DATA REPORT <br />GC Semivolatiles <br />Client Lot #...: E1K150233 Work Order #_..: EN2TLIAH-MS Matrix.........: SOLID <br />MS Lot -Sample #: E1K150233-003 EN2TLlAJ-MSD <br />Date Sampled...: 11/13/01 14:35 Date Received..: 11/15/01 10:35 MS Run #....... : 1319286 <br />Prep Date......: 11/15/01 Analysis Date..: 11/16/01 <br />Prep Batch #...: 1319565 Analysis Time..: 14:17 <br />Dilution Factor: 1 Analyst ID.....: 356074 Instrument ID..: G02 <br />SAMPLE SPIKE MEASRD PERCENT <br />PARAMETER AMOUNT AMT AMOUNT UNITS RECOVERY RPD METHOD <br />TPH (as Diesel) ND 250 200 mg/kg 80 SW846 8015B <br />ND 250 204 mg/kg 82 2.1 SW846 8015B <br />SURROGATE <br />Benzo(a)pyrene <br />PERCENT RECOVERY <br />RECOVERY LIMITS <br />82 (60 - 130) <br />81 (60 - 130) <br />NOTE (S) : <br />Calculations are performed before rounding to avoid round -off errors in calculated results. <br />Bold print denotes control parameters <br />n <br />