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SAN JOAQUIN LOCAr.. HE,' r,TH DISZT•ZIGT <br />TANK CLOSURE PLAN REVIEW CHH LIST - MINIMUM VERIFICATION LAB ANALYSES <br />TANK <br />ID N <br />TANK CONTENTS= <br />Waste Product <br />----�=or _r- <br />_ <br />LEADED GASOLINE <br />TPH-G <br />GC -FID <br />( 5030 ), <br />TPH-D <br />GC -FID <br />TEPH <br />(3550) <br />( 3540 ) <br />BTX&E <br />(8020) <br />CL HC <br />(8010) <br />( 8240 ) <br />TEL EDB <br />(D H S) <br />H& <br />Total Petroleum Hydrocarbon, Diesel <br />METALS <br />(ICP- <br />) <br />PCB <br />(8270) <br />(8080) <br />M HC 8010 OR 8240 <br />TEL (DOHS-LUFT) <br />Chlorinated Hydrocarbon 8010 or 8240 <br />Tetraethyl Lead(DOHS-LUFT) <br />EDB (DOHS -AB 1803) <br />GC FID <br />Ethylene dibromide (DOHS -AB 1803) <br />ICP -AES OR AA <br />- <br />- <br />UNL GASOLINE <br />Purge and Trap Sample Preparation <br />Sonication Sample Preparation <br />DIESEL <br />Soxhlet Sample Preparation <br />Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />Fused capillary columns preferred to columns; a packed column be <br />Mare <br />first cut with dirty <br />proper QA/QC Is followed. <br />tacked may used as a <br />samples or once he hydrocarbons have been characterized and <br />organics be usedkingpreferencertos�hep600eseriesdbecausetthe5detection <br />limItslarellover <br />the QA/QC is better. <br />KEROSENE <br />Z )E'L <br />OIL <br />CHLOR. SOLVENTS <br />NONCHLOR. SOLVTS <br />WASTE/USED OIL=-JIZ: <br />MINIMUM VERIFICATION LABORATORY ANALYSES TERMINOLOGY <br />The following listing of <br />terminology used will be <br />laboratory analyses abbreviations is provided as a guide so that <br />familiar. <br />described in EPA SW 846, <br />more All analyses methods are designated EPA methods as <br />Third Edition. Those methods not found in SW 846, are <br />specifically noted. <br />TPH D Total <br />Petroleum Hydrocarbon, Gasoline <br />H& <br />Total Petroleum Hydrocarbon, Diesel <br />BTXE (8020) <br />Total Extractable Petroleum Hydrocarbon (8015) <br />Benzene, Toluene, Xylene & Ethyl Benzene (8020) <br />M HC 8010 OR 8240 <br />TEL (DOHS-LUFT) <br />Chlorinated Hydrocarbon 8010 or 8240 <br />Tetraethyl Lead(DOHS-LUFT) <br />EDB (DOHS -AB 1803) <br />GC FID <br />Ethylene dibromide (DOHS -AB 1803) <br />ICP -AES OR AA <br />Gas Chromatography Flame Ionization Detector <br />Inductively Coupled Plasma Atomic Emission Spectrometry or Atomic <br />Spectrometry <br />Method 5030 <br />Method 3550 <br />Purge and Trap Sample Preparation <br />Sonication Sample Preparation <br />Method <br />Method 3540 <br />Soxhlet Sample Preparation <br />Quality Assurance/Quality Control <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. <br />Fused capillary columns preferred to columns; a packed column be <br />Mare <br />first cut with dirty <br />proper QA/QC Is followed. <br />tacked may used as a <br />samples or once he hydrocarbons have been characterized and <br />organics be usedkingpreferencertos�hep600eseriesdbecausetthe5detection <br />limItslarellover <br />the QA/QC is better. <br />and <br />SITE ADDRESS�O_ao C, �ikarck . SWEEPS I <br />CONTRACTOR _ SP�I��I�O CanDararhla APPROVAL DATE <br />