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r�uanferra <br /> En+Yronmenral <br /> ` <br /> Services <br /> IATRIX SPIKE/MATRIX SPIKE DUPLICATE QC REPORT <br /> letals Analysis and Preparation <br /> 'roject: 092397 <br /> ..ategory: ICP-S ICP Metals-Ottawa Sand LCS <br /> est ICP-CAMT-LO-S Method: 6010 <br /> iatrix SOIL <br /> ample 092398-0010 <br /> S Run 31 MAR 97-M <br /> nits mg/kg Units Qualifier'Y Wet wt <br /> ---------Concentration--------- r <br /> Amount Acceptance <br /> SampResiult ResDulAt� Ms <br /> dMSD %RMSoveMSD/RPD Limit <br /> Recov. RPD <br /> Analyte Resultr � <br /> �timony ND ' 40.2 41 .9 w 50.0 50.0 80 84 4.2 80-120 50 <br /> irium 44.2 237 238 200 200 96 97 0.58 80-120 50 <br /> �ryllium ND 4.72 4.83 5.00 5.00 94 97 2.3 80-120 50 <br /> idmium -ND 4.69 5.09 _ 5.00 5.00 94 102 8.2 80-120 50 <br /> iromium 4.3 22.3 23.5 20.0 20.0 90 96 5.2 80-120 50 <br /> )bait 3.4 49.7 50.3 50.0 50.0 93 94 1 .3 80-120 50 <br /> ger 113.8 37.4 41 .5 25.0 25.0 94 111 10 80-120.50 ; I <br /> ��ybdenum " ND 94.5 97. 1 100 100 94 97 2. 7 80-120 50 <br /> lckel '6.3 50.5 51 .5 50.0 50.0 89 91 2.0 80-120 50 <br /> ilver ND 4.39 4.55 5.00 5.00 88 91 3 .6 80-120 50 <br /> tnadium 19.3 63.5 64.0 50.0 50.0 88 89 0.83 80-120 50 . <br /> nc 25.9 71 . 1 73.0 50.0 50.0 90 94 2.7 80-120 50 <br /> y <br /> itegory: GFAA10-S Furnace AA Metals a <br /> st AS-QC-FRA-CAMT-S Method: 7060 C <br /> 1rix SOLID <br /> impl a 092398-0001 <br /> Run 29 MAR 97-GA <br /> pits mg/kg Units QualifierY Wet wt. <br /> k <br /> ------Concentration--------- - <br /> Amount Acceptance <br /> Sample '' MS MSD �' Spiked %Recovery %RPD Limit <br /> Analyte Result Result Result M5 MSD MS MSD Recov: RPD <br /> v <br /> �senic 0.877 4.03 4.04 4.00 4.00 79 79 0.25 75-125 20 <br /> .dmium ND 0.206 0.200 0.200 0.200 103 100 3 .0 75-125 20 <br /> xomium 8.94 9.21 10.6 2.00 2.00 NC '' NC NC 75-125 20 <br /> iad 1 .76 3:62 3.85 2.00 2.00 93- 104 6'.2 75-125 20 <br /> lenium ND 1 .48 1 .58 2.00 2.00 74 79 ''6:5 75-125 20 � � <br /> ;allium ND 4.78 4.69 5.00 5.00 96 �94 1"9 75-125. 20 <br /> L <br /> = Not Calculated, calculation not applicable. <br /> = Not Detected 4 r a <br /> , f <br /> lculations are performed before rounding to avoid round-off errors in calculated results. - f� <br />