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it (All-fluantera R Environmenral Services ,TRIX SPIKE/MATRIX SPIKE DUPLICATE QC REPORT I1tals Analysis and Preparation Project: 092397 (cont. ) (,.tegory: ICP-AD ICP Metals / Dissolved �i i Test : ICP-CAMT-AD Method: 6010 Metrix AQUEOUS mple 092525-0001 j Run : 02 APR 97-A Units : mg/L ---------Concentration--------- �� 3 Amount Acceptance ' Sample MS MSD Spiked II %Recovery %RPD Limit 4nalyte Result Result Result MSMSD MS MSD Recov. RPG I Ii knimony NO 0.523 0.538 0.500 0.500 105 108 2.7 80-120 20 ► Arsenic NO 2.06 2.09 2.00 2.00 103 104 1 .4 80-120 20 B rium ND 2.04 2. 12 2.00 2.00 102 106 3.8 80-120 20 L ryllium NO 0.0516 0.0529 0.0500 0.0500 103 106 2.5 80-120 20 Boron 0. 16 1 . 17 1 .21 1 .00, 1'.00 101 105 3 .5 80-120 20 G<'dmium NO 0.0508 0.0504 0.0500 0.0500 102 101 0. 79 80-120 20 C;L 1 ci um 55.0 104 105 50.0 11 50�.0 98 101 1 . 1 80-120 20 C omium NO 0.204 0.206 0.200 0..200 102 103 0.49 80-120 20 Cobalt NO 0. 500 0.513 0.500 0'.500 100 103 2.6 80-120 20 i C aper ND 0.251 0.260 0.250 ' 0.250 100 104 3.1 80-120 20 { I )n NO 1 .05 1 .07 1 .00, 11.00 105 107 2.5 80-120 20 L d NO 0.503 0.479 0.500 0.500 101 96 4.9 80-120 20 Magnesium 9.2 60.8 62.4 50.011 50'.0 103 106 2.5 80-120 20 M-liganese 0.013 0.525 0.537 0.500 0.500 102 105 2. 1 80-120 20 IA ` ybdenum ND 1 .03 1 .05 1 .001 1 .00 103 105 2.0 80-120 20 Nickel ND 0.491 0.513 0.500 0.500 98 103 4.3 80-120 20 Splenium NO 2.03 2.05 2.001 2..00 101 102 1 .2 80-120 20 S ver ND 0.0490 0.0501 0.0500 0;.0500 98 100 2.2 80-120 20 ' S ium 228 276 284 50.0 j 50;.0 NC NC NC 80-120 20 Thallium NO 2.00 NA 2.00:, 2i.00 100 NC NC 80-120 20 V-radium NO 0.496 0.508 0.500 0;.500 99 102 2.3 80-120 20 I ZLIc NO .0.507 0.513 0.500 0;.500 101 103 1 .2 80-120- 20 i N = Not Applicable NC = Not Calculated, calculation not applicable. N-' = Not Detected 4 C culations are performed before rounding to avoid round-off errors in calculated results. j