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WL Certificate of Analysis FINAL REPORT WECK LABORATORIES,INC. Geoanalytical Laboratories,Inc. Project Number: F9J1405 Reported: 2300 Maryann Drive 11/11/2019 15:07 Turlock,CA 95380 Project Manager: Christina Ruiz F Quality Control Results (Continued) Metals(Non-Aqueous)by EPA 6000/7000 Series Methods(Continued) Spike Source %REC RPD Analyte Result MRL Units level Result %REC limits RPD Limit Qualifier Batch: W9.111 606-EPA 6020 (Continued) LCS(W9J 1 606-BS2) Prepared:10/27/19 Analyzed:11/07/19 Barium,Total 49.9 0.50 mg/kg 50.0 100 80-120 Chromium,Total 49.7 1.0 mg/kg 50.0 99 80-120 Molybdenum,Total 46.0 0.50 mg/kg 50.0 92 80-120 Zinc,Total 52.3 5.0 mg/kg 50.0 105 80-120 Matrix Spike(W9J1606-MS1) Source:9124029-02 Prepared:10/27/19 Analyzed:10/30/19 Antimony,Total 8.05 0.50 mg/kg 46.4 0.799 16 75-125 MS-01 Arsenic,Total 47.9 0.50 mg/kg 46.4 2.19 99 75-125 Barium,Total 639 0.50 mg/kg 46.4 162 NR 75-125 MS-01 Beryllium,Total 45.8 0.30 mg/kg 46.4 NO 99 75-125 Cadmium,Total 47.7 0.20 mg/kg 46.4 1.05 101 75-125 Chromium,Total 62.9 1.0 mg/kg 46.4 1B.9 95 75-125 Cobalt,Total 55.2 0.50 mg/kg 46.4 12.0 93 75-125 Copper,Total 192 0.50 mg/kg 46.4 160 69 75-125 MS-D2 Lead,Total 147 0.50 mg/kg 46.4 116 69 75-125 MS-G2 Molybdenum,Total 47,7 0.50 mg/kg 46.4 5.02 92 75-125 Nickel,Total 62.9 1.0 mg/kg 46.4 22.5 87 75-125 Selenium,Total 46.7 0.50 mg/kg 46.4 ND 101 75-125 Silver,Total 45.8 0.50 mg/kg 46.4 1.00 97 75-125 Thallium,Total 49.1 0.50 mg/kg 46.4 ND 106 75-125 Vanadium,Total 126 1.0 mg/kg 46.4 81.0 97 75-125 Zinc,Total 452 5.0 mg/kg 46.4 357 206 75-125 MS-C2 Matrix Spike(W9J1606-MS2) Source:9.124029-02 Prepared:10/27/19 Analyzed:11/07/19 Barium,Total 711 2.5 mg/kg 50.0 162 NR 75-125 MS-C2 Chromium,Total 69.0 5.0 mg/kg 50.0 18.9 100 75-125 Molybdenum,Total 49.4 2.5 mg/kg 50.0 5.02 89 75-125 Zinc,Total 562 25 mg/kg 50.0 357 410 75-125 MS-C2 Matrix Spike Dup(W9J1606-MSD1) Source:9124029-02 Prepared:10/27/19 Analyzed:10/30/19 Antimony,Total 10.0 0.50 mg/kg 49.1 0.799 19 75-125 22 20 MS-C 1 Arsenic,Total 47.7 0.50 mg/kg 49.1 2.19 93 75-125 0.4 20 Barium,Total 177 0.50 mg/kg 49.1 162 30 75-125 113 20 MS-C 1 Beryllium,Total 47.4 0.30 mg/kg 49.1 ND 97 75-125 3 20 Cadmium,Total 48.9 0.20 mg/kg 49.1 1.05 97 75-125 2 20 Chromium,Total 69.6 1.0 mg/kg 49.1 18.9 103 75-125 10 20 Cobalt,Total 55.9 0.50 mg/kg 49.1 12.0 90 75-125 1 20 Copper,Total 164 0.50 mg/kg 49.1 160 8 75-125 16 20 MS-(2 Lead,Total 141 0.50 mg/kg 49.1 116 52 75-125 4 20 MS-C2 Molybdenum,Total 49.2 0.50 mg/kg 49.1 5.02 90 75-125 3 20 Nickel,Total 58.5 1.0 mg/kg 49.1 22.5 73 75-125 7 20 MS-(1 Selenium,Total 47.7 0.50 mg/kg 49.1 ND 97 75-125 2 20 9124044 `.]v 5 of 140,:i9'lark A.v.=nue.C'ty of Industry G:.91746 i Phone''.(6,61 336-213!' i F;ax.(526)3.'s6-2634 eve-•w.wo,klabs.CAM