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WCertificate of Analysis FINAL REPORT WECK LABORATORIES,INC. Geoanalytical Laboratories,Inc. Project Number: F9J1405 Reported: 2300 Maryann Drive 11/11/2019 15:07 Turlock,CA 95380 Project Manager: Christina Ruiz Quality Control Results (Continued) Metals(Non-Aqueous)by EPA 6000/7000 Series Methods(Continued) Spike Source %REC RPO Analyte Result MRL Units Level Result %REC Limits RPD Limit Qualifier Batch: W9.1111 606-EPA 6020 (Continued) Matrix Spike Dup(W9J1606-MSD1) Source:9.124029-02 Prepared:10/27/19 Analyzed:10/30/19 Silver,Total 46.4 0.50 mg/kg 49.1 1.00 93 75-125 1 20 Thallium,Total 49.8 0.50 mg/kg 49.1 ND 102 75-125 1 20 Vanadium,Total 120 1.0 mg/kg 49.1 81.0 80 75-125 5 20 Zinc,Total 334 5.0 mg/kg 49.1 357 NR 75-125 30 20 MS-0.1 Matrix Spike Dup(W9J 1 606-MSD2) Source:9.124029-02 Prepared:10/27/19 Analyzed:11/07/19 Barium,Total 178 2.5 mg/kg 50.0 162 32 75-125 120 20 MS-02 Chromium,Total 74.8 5.0 mg/kg 50.0 18.9 112 75-125 8 20 Molybdenum,Total 49.0 2.5 mg/kg 50.0 5.02 88 75-125 0.9 20 Zinc,Total 402 25 mg/kg 50.0 357 90 75-125 33 20 MS-0.= Post Spike(W9.11606-PSI) Source:9.124029-02 Prepared:10/27/19 Analyzed:10/30/19 Antimony,Total 0.0478 mg/I 0.0500 0.000799 94 80-120 Barium,Total 0.220 mg/I 0.0500 0.162 115 80-120 Copper,Total 0.211 mg/I 0.0500 0.160 102 80-120 Zinc,Total 0.424 mg/I 0.0500 0.357 134 80-120 Post Spike(W9.11606-PS2) Source:9.124029-02 Prepared:10/27/19 Analyzed:10/30/19 Antimony,Total 0.0476 mg/I 0.0500 0.000799 94 80-120 Barium,Total 0.222 mg/I 0.0500 0.162 119 80-120 Copper,Total 0.214 mg/I 0.0500 0.160 108 80-120 Nickel,Total 0.0672 mg/I 0.0500 0.0225 89 80-120 Zinc,Total 0.426 mg/I 0.0500 0.357 138 80-120 9124044 f 149 Clark Avenue.0 ity of Industry CA 9'7-45 Phon•s:(626) Ei .'.1 i4 Fax:(526)336-2634 v:w;v.weckl:�bs c.�rn