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Appendix E.1:Data Usability Summary <br /> evaluated when the sample was diluted by a factor of 10 or more, and are considered"diluted <br /> out." All surrogates were within laboratory control limits with the following exceptions: <br /> • The %R for orthoterphenyl was 265 percent, above the lab control limit of 129 percent, in <br /> sample SB-28-S-43-081124. The result was qualified E for a possible high bias. <br /> • The %R for orthoterphenyl was 143 percent, above the lab control limit of 129 percent, in <br /> sample SB-22-S-53-080813. The result was qualified E for a possible high bias. <br /> • The %R for orthoterphenyl was 143 percent, above the lab control limit of 129 percent, in <br /> sample SB-25-S-47-080818. The result was qualified E for a possible high bias. <br /> Field Duplicate <br /> Groundwater field duplicates SB-22-WD-080813 (duplicate of SB-22-W-080813), DUP-I-WD- <br /> 081120 (duplicate of SB-37-W-35-081120), and SB-42-WD-090305 (duplicate of SB-42-W- <br /> 090305)were submitted as part of this data set. RPDs were calculated for analytes that were <br /> detected in both the field duplicate and parent sample. All calculated RPDs were below the <br /> control limit of 30 percent with the following exceptions: <br /> • The RPDs for TPHd, TPHd with silica gel, naphthalene, acenaphthene, anthracene, <br /> fluoranthene,pyrene, and benzo(b)fluoranthene, calculated for the results reported in <br /> sample SB-22-W-080813 and field duplicate SB-22-WD-080813, were above 30 percent. <br /> The results were qualified E in the sample and field duplicate. <br /> • The RPD for acenaphthylene, calculated for the results reported in sample SB-37-W-35- <br /> 081120 and field duplicate DUP-I-WD-081120, was above 30 percent. The results were <br /> qualified E in the sample and field duplicate. <br /> • Acenaphthene and fluorene were not detected in sample SB-37-W-35-081120; however, <br /> the compounds were detected above the program reporting limits in field duplicate <br /> DUP-I-WD-081120. TPHd were detected in sample SB-37-W-35-081120, but not in the <br /> field duplicate. The results were qualified E in the sample and field duplicate. <br /> • Pyrene was not detected in sample SB-42-W-090305, but the compound was detected in <br /> the field duplicate SB-42-WD-090305. PAHs benzo(a)anthracene, chrysene, <br /> benzo(b)fluoranthene, benzo(k)fluoranthene,benzo(a)pyrene, and dibenz(a,h)anthracene <br /> were detected in sample SB-42-W-090305, but not in the field duplicate. The results <br /> were qualified E as estimated. <br /> MS/MSDs <br /> Two project-specific MS/MSD samples were collected with samples as part of this data set. The <br /> laboratory also randomly selected several project samples to prepare MS/MSD samples with <br /> some batches of samples. The samples in this data set were not evaluated in terms of the <br /> recoveries of the non-project MS/MSDs because they are not likely representative of the same <br /> sample matrix. The recoveries of the MS and MSD samples evaluated were within laboratory <br /> control limits with the following exceptions: <br /> E.1-4 <br /> From Science to Solutions <br />