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Matrix Spike/Matrix Spike Duplicate Summary 1"u-'e 1 of 1 <br /> Job Number: C15380 <br /> Account: TERRACAI Terracon <br /> Project: Love's Travel LS1 - Highway 12, Lodi, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> OP3691-MS GG23427.D 1 04/02/11 JH 04/01/11 OP3691 GGG653 <br /> OP3691-MSD GG23428.D 1 04/02/11 JH 04/01/11 OP3691 GGG653 <br /> C15094-7A a GG23415.D 1 04/02/11 JH 04/01/11 OP3691 GGG653 — <br /> The QC reported here applies to the following samples: Method: SW846 8015B M <br /> C15380-1, C15380-2, C15380-3 <br /> C15094-7A Spike MS MS MSD MSD Limits <br /> CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg % RPD Rec/RPD <br /> TPH (C10-C28) ND 100 76.1 76 77.0 77 1 45-140/30 <br /> TPH (> C28-C40) ND 100 80.5 81 82.2 82 2 45-140/30 <br /> CAS No. Surrogate Recoveries MS MSD C15094-7A Limits <br /> 630-01-3 Hexacosane 92% 89% 81% 45-140% <br /> (a) Sample received outside the holding time. <br /> 39 of 40 <br /> ACCUTEST <br /> C15380 •eO <br />