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Matrix Spike/Matrix Spike Duplicate Summary Page I of 1 <br /> Job Number: C15380 <br /> Account: TERRACAI Terracon <br /> Project: Love's Travel LS1 -Highway 12, Lodi, CA <br /> Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch <br /> OP3693-MS GG23525.13 1 04/06/11 JH 04/04/11 OP3693 GGG655 <br /> OP3693-MSD GG23526.D 1 04/06/11 JH 04/04/11 OP3693 GGG655 w <br /> C15390-4 GG23442.D 1 04/04/11 MT 04/04/11 OP3693 GGG654 iv <br /> The QC reported here applies to the following samples: Method: SW846 8015B M <br /> C15380-6, C15380-7, C15380-8 <br /> C15390-4 Spike MS MS MSD MSD Limits <br /> CAS No. Compound mg/I Q mg/I mg/1 % mg/I % RPD Rec/RPD <br /> TPH (C10-C28) ND 2.13 1.97 93 1.95 92 1 45-140/25 <br /> TPH (> C28-C40) ND 2.13 1.79 84 1.74 82 3 45-140/25 <br /> CAS No. Surrogate Recoveries MS MSD C15390-4 Limits <br /> 630-01-3 Hexacosane 90% 88% 81% 45-140% <br /> ■ 40 of 40 <br /> ■ACCIJTEST <br /> C15380 "" <br />