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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project:PG5 <br /> 10011 Street Project Number: 2512 Vineyard Ave Reported: <br /> Sacramento CA,95814 Project Manager: Glenn Young 10-May-13 14:39 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A304778-EPA TO-15 prep <br /> Blank(A304778-BLKI) Prepared&Analyzed:30-Apr-13 <br /> Isopropyl alcohol ND 0.50 ppbv <br /> Methylene chloride ND 0.50 " <br /> Methyl Ethyl Ketone ND 0.50 " <br /> Methyl Isobutyl Ketone ND 0.50 " <br /> Methyl-t-butyl ether ND 0.50 " <br /> Propylene ND 0.50 " <br /> Styrene ND 0.50 " <br /> t-Amyl Methyl Ether ND 0.50 " <br /> t-Butyl alcohol ND 0.50 " <br /> 1,1,2,2-Tetrachloroethane ND 0.50 " <br /> Tetrachloroethene(PCE) ND 0.50 <br /> Tetrahydrofuran ND 0.50 <br /> Toluene ND 0.50 " <br /> 1,2,4-Trichlorobenzene ND 0.50 " <br /> 1,1,1-Trichloroethane ND 0.50 " <br /> 1,1,2-Trichloroethane ND 0.50 " <br /> Trichloroethene(TCE) ND 0.50 " <br /> Trichlorofluoromethane ND 0.50 " <br /> 1,1,2-Trichlorotrifluoroethane ND 0.50 " <br /> 1,2,4-Trimethylbenzene ND 0.50 " <br /> 1,3,5-Trimethylbenzene ND 0.50 " <br /> Vinyl acetate ND 0.50 " <br /> Vinyl chloride ND 0.50 " <br /> Xylenes(total) ND 0.50 " <br /> LCS(A304778-BSI) Prepared&Analyzed:30-Apr-13 <br /> Benzene 9.46 0.50 ppbv 10.0 94.6 63-130 <br /> Bromomethane 10.4 2.0 10.0 104 12-233 <br /> Carbon tetrachloride 9.96 0.50 10.0 99.6 61-130 <br /> Chlorobenzene 9.18 0.50 10.0 91.8 69-123 <br /> Chloroform 9.65 0.50 10.0 96.5 56-144 <br /> 1,2-Dibromoethane(EDB) 9.29 0.50 10.0 92.9 58-141 <br /> 1,3-Dichlorobenzene 8.76 0.50 10.0 87.6 34-182 <br /> 1,4-Dichlorobenzene 8.77 0.50 10.0 87.7 46-175 <br /> Dichlorodifluoromethane 10.3 0.50 10.0 103 53-168 <br /> 1,2-Dichloroethane 10.0 0.50 10.0 100 57-154 <br /> 1,1-Dichloroethene 9.66 0.50 10.0 96.6 43-163 <br /> 1,2-Dichloropropane 9.68 0.50 10.0 96.8 61-130 <br /> Diisopropyl Ether 9.80 0.50 10.0 98.0 0-200 <br /> Ethanol 10.4 0.50 10.0 104 28-177 <br /> Ethylbenzene 8.23 0.50 10.0 82.3 53-139 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples anal),-ed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 58 of 72 <br />