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Oilfield Environmental and Compliance, INC. <br /> CalRecycle Project:PG5 <br /> 1001 I Street Project Number: 2512 Vineyard Ave Reported: <br /> Sacramento CA,95814 Project Manager: Glenn Young 10-May-13 14:39 <br /> Volatile Organic Compounds by EPA Method TO-15-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A304778-EPA TO-15 prep <br /> LCS(A304778-BSI) Prepared&Analyzed:30-Apr-13 <br /> Ethyl t-Butyl Ether 9.85 0.50 ppbv 10.0 98.5 0-200 <br /> Methylene chloride 9.90 0.50 10.0 99.0 29-190 <br /> Methyl-t-butyl ether 10.1 0.50 10.0 101 58-145 <br /> Styrene 9.72 0.50 10.0 97.2 61-141 <br /> t-Amyl Methyl Ether 9.76 0.50 10.0 97.6 0-200 <br /> t-Butyl alcohol 9.76 0.50 10.0 97.6 0-200 <br /> Tetrachloroethene(PCE) 9.03 0.50 10.0 90.3 61-131 <br /> Toluene 7.65 0.50 10.0 76.5 60-131 <br /> 1,1,1-Trichloroethane 10.1 0.50 10.0 101 59-140 <br /> Trichloroethene(TCE) 9.63 0.50 10.0 96.3 66-131 <br /> Trichlorofluoromethane 10.1 0.50 10.0 101 52-155 <br /> Vinyl chloride 10.9 0.50 10.0 109 26-197 <br /> Xylenes(total) 25.8 0.50 30.0 86.0 60-139 <br /> LCS Dup(A304778-BSDI) Prepared:30-Apr-13 Analyzed:01-May-13 <br /> Benzene 9.75 0.50 ppbv 10.0 97.5 63-130 3.02 25 <br /> Bromomethane 10.4 2.0 10.0 104 12-233 0.481 25 <br /> Carbon tetrachloride 10.0 0.50 10.0 100 61-130 0.900 25 <br /> Chlorobenzene 10.2 0.50 10.0 102 69-123 10.1 25 <br /> Chloroform 10.2 0.50 10.0 102 56-144 5.44 25 <br /> 1,2-Dibromoethane(EDB) 10.2 0.50 10.0 102 58-141 9.04 25 <br /> 1,3-Dichlorobenzene 9.62 0.50 10.0 96.2 34-182 9.36 25 <br /> 1,4-Dichlorobenzene 9.09 0.50 10.0 90.9 46-175 3.58 25 <br /> Dichlorodifluoromethane 10.6 0.50 10.0 106 53-168 3.63 25 <br /> 1,2-Dichloroethane 10.2 0.50 10.0 102 57-154 1.98 25 <br /> 1,1-Dichloroethene 9.90 0.50 10.0 99.0 43-163 2.45 25 <br /> 1,2-Dichloropropane 10.1 0.50 10.0 101 61-130 3.95 25 <br /> Diisopropyl Ether 10.2 0.50 10.0 102 0-200 4.29 25 <br /> Ethanol 9.01 0.50 10.0 90.1 28-177 14.6 25 <br /> Ethylbenzene 9.48 0.50 10.0 94.8 53-139 14.1 25 <br /> Ethyl t-Butyl Ether 9.96 0.50 10.0 99.6 0-200 1.11 25 <br /> Methylene chloride 10.1 0.50 10.0 101 29-190 2.20 25 <br /> Methyl-t-butyl ether 10.0 0.50 10.0 100 58-145 0.794 25 <br /> Styrene 10.7 0.50 10.0 107 61-141 9.32 25 <br /> t-Amyl Methyl Ether 9.86 0.50 10.0 98.6 0-200 1.02 25 <br /> t-Butyl alcohol 9.90 0.50 10.0 99.0 0-200 1.42 25 <br /> Tetrachloroethene(PCE) 9.63 0.50 10.0 96.3 61-131 6.43 25 <br /> Toluene 8.27 0.50 10.0 82.7 60-131 7.79 25 <br /> 1,1,1-Trichloroethane 10.3 0.50 10.0 103 59-140 1.96 25 <br /> Trichloroethene(TCE) 9.98 0.50 10.0 99.8 66-131 3.57 25 <br /> Trichlorofluoromethane 10.0 0.50 10.0 100 52-155 0.796 25 <br /> Oilfield Environmental and Compliance The results in this report apply to the samples analysed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> TEL: (805) 922-4772 <br /> 307 Roemer Way, Suite 300, Santa Maria, CA 93454 www.oecusa.com FAX: (805) 925-3376 <br /> Page 59 of 72 <br />