Laserfiche WebLink
sampling for volatile organics. These bottles are filled completely to prevent air from remaining in the <br /> bottle. A positive meniscus forms when the bottle is completely full. A convex Teflon septum is <br /> placed over the positive meniscus to eliminate air. After the bottle is capped, it is inverted and tapped <br /> to verify that it contains no air bubbles. <br /> Dissolved Metals <br /> To determine dissolved concentrations of metals, appropriate field filtration techniques are used. <br /> When using a Teflon bailer, the sample is filtered by emptying the contents of the bailer into a <br /> pressure transfer vessel. A disposable 0.45-micron acrylic copolymer filter is threaded onto the <br /> transfer vessel at the discharge point and the vessel is sealed. Pressure is applied to the vessel <br /> with a hand pump and the filtrate is directed into the appropriate containers. Each filter is used <br /> once and discarded. <br /> When using a bladder pump to collect samples for dissolved constituents, the sample is filtered by <br /> attaching a disposable 0.45-micron acrylic copolymer filter directly to the pump effluent line with <br /> a pressure fitting. As the pump cycles, the effluent is pressured through the filter and directed into <br /> the appropriate containers. Each filter is used once and discarded. <br /> Spring (or Surface Water) Sampling <br /> If sufficient flow is observed, spring(or surface water) samples are collected with a dipper consistent <br /> with the procedures listed in Section 9 of "Test Methods for Evaluating Solid Waste: <br /> Physical/Chemical Methods," SW-846, 3rd edition, November 1986. If low-flow conditions are <br /> encountered,a stainless steel scoop is used to collect samples. The flat bottom of the scoop is pressed <br /> against the bank and the water will flow with little disturbance into the scoop. Samples collected with <br /> a dipper or scoop are transferred into the appropriate sample containers. Spring (or surface water) <br /> samples are filtered as required. <br /> Leachate Sampling <br /> If leachate sampling and analysis is required, samples are collected after purging approximately <br /> one casing volume using a Teflon bailer. Leachate samples are filtered as required and transferred <br /> into the appropriate containers. <br /> Lysimeter Sampling <br /> If lysnneter sampling and analysis is required, a vacuum is applied to the lysnneter only if an <br /> electrical conductivity monitor indicates that the soil-moisture content and soil suction are adequate <br /> for attempting to collect a sample. Vacuum and pressure is alternately applied to lysimeter over a <br /> 72-hour period to achieve the sample volume required for analysis. If sufficient sample volume is not <br /> Groundwater Monitoring A-4 Department of Public Works/Solid Waste <br /> County of San Joaquin <br />