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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' 24 h //www mccam bell com E-mail main@mccampbell com <br /> • <br /> Advanced GeoEnvironmental Client Project ID Waterloo Food&Fuel Date Sampled 10/31-11/02/01 <br /> 837 Shaw Road Date Received 11/06/01 <br />' Stockton, CA 95215 Client Contact Bill Little Date Extracted 11/06/01 <br /> Client P O Date Analyzed 11/07-11/09/01 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* &BTEX* <br /> EPA methods 5030,modified 9015,and 8020 or 602,California RWQCB(SF Bay Region)method GCFID(5030) <br />' + Ethyl- %Recovery <br /> Lab 1D benzene Surrogate <br /> Client 1D Matrix TPEI(g} MTBE Benzene Toluene Xylenes <br /> 82776 MW7B/110201 W 2600,a ND<35 140 390 82 480 102 <br />' 82777 MW7C/ W 830,a ND<15 110 160 15 77 102 <br /> 110201 <br /> 82778 MW7D/ W 990,a ND<15 74 180 25 130 100 <br />' 110201 <br /> 82779 MW7E/ W 140,a ND 95 26 3 0 13 105 <br /> 1I0201 <br /> 82780 E 10 SA W ND,t ND ND 082 066 3 3 100 <br /> 82781 MW8B/ W ND ND ND ND ND 15 100 <br /> 110201 <br /> 82782 MW8C/ W ND,t ND ND 079 0 78 3 8 101 <br /> 110201 <br /> 82783 MW8D/ W ND,i ND ND 0 96 ND 1 6 101 <br /> 110201 <br /> 82784 MW8E/ W ND ND ND ND ND ND 101 <br /> 110201 <br /> r <br /> Reporting Limit unless W 50 ug/L 5 0 0 5 0 5 05 0 5 <br /> otherwise stated,ND <br /> means not detected above <br /> the reporting limit m S 1 0 /k 005 0 005 0 005 0 005 0 005 <br /> mg/kg <br /> 'water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br /> A cluttered chromatogram,sample peak coelutes With surrogate peak <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant b) heavier gasoline range compounds are signi8cant(aged <br /> gasoline"), c) lighter gasoline range compounds (the most mobile fraction) are significant d) gasoline range compounds having broad <br /> . chromatographic peaks are significant,biologically altered gasolmO e)TPM pattern that does not appear to be derived from gasoline(9), f) <br /> one to a few isolated peaks present,g) strongly aged gasoline or diesel range compounds are significant, h)lighter than water immiscible <br /> Sheen is present,i)liquid sample that contains greater than—5 vol %sediment,j)no recognizable pattern <br /> DHS Certification No 1644 Edward Hanulton, Lab Director <br /> I <br />