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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCANIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htt�_//www mccampbell corn E-mail main@mccampbelI com <br /> Advanced GeoEnvironmental Client Project ID Waterloo Food&Fuel Date Sampled 1 013 1-1 110210 1 <br /> 837 Shaw Road Date Received 11/06/01 <br />' Stockton, CA 95215 Client Contact Bill Little Date Extracted 11/08-11112101 <br />' Client P O Date Analyzed 11/08-11/12/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 82762 82763 82764 82765 <br /> MWI/ MW2/ MW3/ W4/ Reporting Linut <br /> Client 11) M <br /> 110101 110201 110101 110101 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg uglL <br /> Di-isopropyl Ether(RIPE) ND<50 ND<2500 ND<2500 ND<2500 50 10 <br />' Ethyl tent-Butyl Ether(ETBE) ND<50 ND<2500 ND<2500 ND<2500 50 1 0 <br /> lieMethyl tert-Butyl Ether(MTBE) 2000 110,000 63,000 150,000 50 1 0 <br /> tent-Amyl Methyl Ether(TAME) ND<50 ND<2500 ND<2500 ND<2500 50 10 <br /> tert-Butanol ND<250 ND<12,500 ND<12,500 ND<12,500 25 50 <br />' Methanol ND<25,000 ND<1,250,000 ND<1,250,000 ND<1,250,000 2500 500 <br /> Ethanol ND<2500 ND<125,000 ND<125,000 ND<125,000 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 114 110 108 1 <br /> 07 <br /> Comments h,i h h i <br /> *water samples are reported in ug/L,sod and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> Ihigh organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />