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01/03/2002 13:54 2094671,x.18 AGE STOCKTON PAGE 04 <br /> t 9 � • <br /> MCCAMPBELL ANALYTICAL INC. 1 I o 2nd Aveoue south,#D7,Pacheco,CA 94553-5560 <br /> Te]ephone;925-798-1620 Fax:925J98-]622 <br /> tt ://wlvw.mceamobe�com E-mail:mainQmccatrtpbell.com <br /> Advanced GeoEnvironmental Client Project ID: Top Filling Date Sampled: 12/11/01 <br /> 837 Shaw Load Date Received: 12/12/01 <br /> Stockton, CA 95215 Client Contact:Tim Cuellar <br /> Date Extracted: 12120.12/21/01 <br /> Client P.O. Date Analyzed; <br /> EPA method 8260 modified Seven Oxygenated Volatile Organics By GC/MS <br /> Lab ID 86153 86154 <br /> 86155 86156 <br /> Client ID Mµ'5/ MW6A/ MW6B/ MW6C Reporting Limit <br /> 121101 121101 121101 121101 <br /> Matrix W W <br /> W W S W <br /> Compound cc <br /> 5p-7 o Cog4eyt atior"0-SS 1160[9 ug/L <br /> 4> 7 70--7S <br /> Di-isopropyl Ether(DIPE) ND ND<250 ND<5.0 <br /> ND 5.0 LO <br /> Ethyl Cert-Butyl Ether(ETBE) ND N1j<250 ND<5.0 ND <br /> 5.0 1.0 <br /> Methyl tert-Butyl Ether(MTBE) ND r-'2116W 240 <br /> 1,2 5.0 1.0 <br /> terl-Amyl Methyl Ether(TAME) ND ND<250 ND<5.0 <br /> ND 5.0 1.0 <br /> tert-Butanol ND ND<1250 ND<25 ND 25 5.0 <br /> Methanol ND ND<125,000 N250 ND 2500 500 <br /> Ethanol ND ND<12,500 ND<250 ND 250 50 <br /> Surropte Recoveries(%) <br /> Dibrumotluoromethene 110 104 95 111 <br /> Comments: <br /> "water samples are reported in ug/1„soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/$TLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.o/u sediment;6)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />