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03/03/2002 13: 54 2094671],18 AGE STOCKTON . PAGE 05 <br /> a <br /> ® MCCA;BPLL AN10 2nd Avenue South,#D7,pacheco,CA 94553-5560 <br /> ALYTICAL INC.IVCTelephone:925.798-1620 Fax:925-798.1622 <br /> ://www mcramnbelt`om E-mail:mainQmccwMbell.com <br /> Advanced GeoEnvironmeatal Client Project ID:Top Filling Date Sampled: 12/11/01 <br /> 837 Shaw Road Date Reocived: 12/12/01 <br /> Stockton,CA 95215 Client Contact:Tim Cuellar Date Extracted: 12/2042/21/01 <br /> Client PA: Date Analyzed: 12120-12/2I/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> LAbID 86157 86158 86159 86160 <br /> Chant ID MW6W MW6E/ MW7E/ MW7C/ RepoltmgLirnit <br /> 121101 121101 121101 121101 <br /> Matrix W W W W S W <br /> Compound fOS-I1 U 15-1 �50_S5 ?p_75 uFJkg ueL <br /> DWsopropyl Ether(DIPS) ND ND ND<5.0 ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND<5.0 ND 5.0 1.0 <br /> Methyl tert-Butyl Ether(MTBE) 1.1 ND 320 ND 5.0 1.0 <br /> tent-Amyl Methyl Ether(TAME) ND ND ND<5.0 ND 5.0 1.0 <br /> tert-Butanol ND ND ND<25 ND 25 5.0 <br /> Methanol ND ND NDK2500 ND 2500 500 <br /> Ethanol ND ND ND<250 ND 250 So <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 115 116 84 110 <br /> Comments: <br /> +water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting litrut;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible shean is present;(i)liquid sample that contains greater than—5 val.%sediment;d)aatnple diluted due to <br /> high organic content <br /> DHS Certification No. 1644 it <br /> .Edward Hamilton,Lab Director <br />