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0'1/03/2002 13:54 2094678 AGE STOCKTON <br /> • PAGE 07 <br /> MCCAWRELL ANALYTICAL INC. 11 Teld honeu 925-798eSou #D7,Pacheco,CA 94553-5560 <br /> C� 1620 leax:925-798.1622 <br /> ://tv<vtv.tnccam,�bell cam E-mail: ocampbell.com <br /> Advanced GeoEnvironmental Client Project ID: Top)tilling Date Sampled; 12/11/01 <br /> 837 Shaw Road <br /> Date Received: 12/12/01 <br /> Stockton,CA 95215 Client Contact:Tim Cuellar <br /> Date Extracted: 12/20-12/21/01 <br /> Client p,O: Date Analyzed: 12/20.12/21/01 <br /> EPA method 8260 modified Seven Oxygenated Volatile Organlcl By GC/MS <br /> Lab ID 86165 860166 <br /> Clientlr) VW2A/ VW3A/ Reporting Limit <br /> 121101 111101 <br /> Matrix W W <br /> 8 W <br /> Compound <br /> ' <br /> 3—(0 f3 .'it5 entration+ ngft ug/L <br /> Di-isopropyl Ether(DrPE) NIK5.0 ND <br /> 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND<5.0 ND <br /> 5.0 1.0 <br /> Methyl tert-Butyl Ether(MTBE) 550 110 <br /> 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND<5.0 ND <br /> 5.0 1.0 <br /> tett-Butanol 83 ND <br /> 25 5.0 <br /> Methanol ND<2500 ND <br /> zsoli sDD <br /> Ethanol ND<500 ND<100 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluommethane 104 109 <br /> Comments: <br /> +water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLp extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)simple diluted due to <br /> high organic concent <br /> DHS Certification No, 1644 Edward Hamilton,Lab Director <br />