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03/03/2002 13:54 2094678 AGE STOCKTON • PAGE 06 <br /> 4EEE <br /> HE <br /> 110 2nd Telephone:925-798-1620P Faxx92CA <br /> 79851622560 <br /> h :1/wWw.mccamobell com E-mail:mein@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Top Filling Date Sampled: 12/11/01 <br /> 837 Shaw Road Date Received: 12/12/01 <br /> Stockton,CA 95215 Client Contact: Tim Cuellar Date Extracted: 12/20.12/21/01 <br /> Client P.O: Date Analyzed: 12/20-12/21/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> LPA method 8260 modified <br /> Lab ID 86161 86162 86163 86164 <br /> Client ID MW7D/ MW7E/ VW1B/ --VW—JC/ FxPortnts Limit <br /> 121101 121101 121101 121101 <br /> Matrix W W W W 5 W <br /> CompoundOS_110 ,, C1,17"""1'0503 <br /> en""1'05 —`f3 -63 as/k8 up/L <br /> Di-isopropyl Ether(RIPE) ND ND NDa5.0 ND<5.0 5.0 1.0 <br /> Ethyl tent-Butyl Ether(ETBE) ND ND ND<5.0 ND<5.0 5.0 1.0 <br /> Methyl tort-Butyl Ether(MTBE) ND ND 200 82 5.0 1.0 <br /> tent-Amyl Methyl Ether(TAME) ND ND ND<5.0 ND<5.0 5.0 1.0 <br /> tent-Butanol ND ND ND<25 ND<25 25 5.0 <br /> Methanol ND ND ND<2500 ND<2500 2500 500 <br /> Ethanol ND ND ND<250 ND<500 250 so <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 114 115 95 104 <br /> Comments: <br /> water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L. <br /> ND means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> (h)tighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment; <br /> (j)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />