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n, <br /> 110 2nd Avenue South,#fD7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hnp.//www mr-,camp ell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Protect ID Top Filling Date Sampled 06/14/99 <br /> 4005 North Wilson Way Date Received 06/17/99 <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06119-06/22/99 <br /> [Client P O Date Analyzed 06/19-06/22199 <br /> Oxygenated Volatile Organics By GCIMS <br /> EPA method 8260 modified <br /> Lab 1D 13440 13441 13442 13443 <br /> MW-1/6-I4- MW-2/1-14- MW-316-14- MW-516-14- Reporting Limit <br /> Client ID 99 99 99 99 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND ND 50 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 10 <br /> Methyl-tert Butyl Ether(MTBE) ND 14 7 8 ND 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 50 1 0 <br /> tent-Butanol ND ND ND 42 25 so <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 108 109 107 108 <br /> Comments <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,%lipes in ug/wipe and all TCLP/STLC/SDLP extracts in ug/L <br /> ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 1—�I—L_Edward Hamilton, Lab Director <br /> I <br />