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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> u McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hUp//www„Mp&gmpl;tfll.com E-mail main@mccampbcll com <br /> Advanced GeoEnvironmental Client Project ID Top FilImg Date Sampled 06/14/99 <br /> 4005 North Wilson Way Date Received 06/17/99 <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 06119-06/22/99 <br /> [Client P O Date Analyzed 06119-06/22/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 13444 13445 13446 <br /> VW-116-14- VW-2/6-14- VW-316-14- Reporting Limit <br /> Client ID 99 99 99 <br /> Matrix W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(RIPE) ND<100 ND<50 ND<25 50 10 <br /> Ethyl Cert-Butyl Ether(ETRE) ND<100 ND<50 ND<25 50 1 0 <br />. Methyl-ten Butyl Ether(MTBE) 850 1200 900 50 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<100 ND<50 ND<25 50 1 0 <br /> tert-Butanol ND<500 250 ND<130 25 50 <br /> Surrogate Recoveries(%) <br /> Dihromofluoromethane 109 107 108 <br /> Comments J J J <br /> *NN ater samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the repotting limit,N/A means surrogate not apphcable to this analysis <br /> (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol %sediment,(i)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />