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I <br /> 110 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> 1 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 6 44 <br /> t /www E-mail main@mccampbell com <br />' Advanced GeciEnvironmontal ClDate Sampled 06/12/98 <br /> Client Project 1D Top Filling <br />' 4005 North Wilson Way Date Received 06/17/98 <br /> Stockton, CA 95205 Client Contact Tim Cuellar Date Extracted 06/19-06/20/98 <br />' Client P O Date Analyzed 06119-06/20/98 <br /> EPA method 8260 Volatile Organics By GC/MS <br />' Lab ID 90576 <br /> Client 1D MW3/6-12-98 <br /> Matrix W <br />' Compound Concentration* Compound Concentration* <br /> Acetone' ND< Ethylbenzene ND <br /> Benzene 17 Hexachlorobuladiene ND <br />' Bromobeozene ND lodomethane ND <br /> B-rmochloromethane ND Isopiopylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromofonn ND Methyl butyl ketone' ' ND <br />' Bromomethane ND Methylene Chloi ide"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Bury]benzene ND Methyl isobutyl ketone`6 ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND St}rene' ' ND <br /> Chloroethane ND 1,1,12-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1 1 2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Clilorotoluene ND 1 2 3 Tnchlorobenzene ND <br /> 4-Chlorotoluene ND 12,4-Trichlorobenzene ND <br /> Dibromochloromethane ND I 1 1-1 i ichloroethane ND <br /> 1 2-Dibromo-3-chloropropane ND 1 1 2-TrtehlOrMthane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorolluoromethane ND <br /> 1,3-Dichlorobenzene ND 12,3-Trichloropropane ND <br /> I 4-Dichlorobenzene ND 1 2 4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 13,5-Tri methyl benzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate"°' ND <br /> 1,2-Dichloroethane 22 Vinyl Chloride"' ND <br /> 1,1-Dichloroethene ND Xylenes total 10' ND <br /> cis-1,2-Dtchloroetbene ND <br />' <br /> Trans-l,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1 3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dtchloropropene ND Surrogate Recd%cries(%) <br /> cis-1,3-Dichloropropene ND Dibroniotluoromethane 109 <br /> trans-l,3-Dichloropropene ND Toluene-d8 104 <br /> Ethylene dibromide ND 4-13romofluorobenzene 46 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes to ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L vapor samples 05 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton,Lab Director <br />