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r <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mcca�nbell com E-mail main@mccampbell com <br /> Date Sampled 06/12/98 <br /> Advanced GeoEnvironmcntal Client Project ID Top Filling <br /> 4005 North Wilson Way Date Received 06/17/98 <br /> Stockton, CA 95205 Client Contact Tun Cuellar Date Extracted 06/19-06120/98 <br /> IClient P O Date Analyzed 06/19-06/20/98 <br /> EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 90577 <br /> Client ID MW4/6-12-98 <br /> Matrix W <br /> I Compound Concentration* Compound Concentration* <br /> Acetone ND<2 Ethylbenzene ND <br /> Benzene ND Hexachlorobuiadiene ND <br /> Bromobenzene ND Iodomethane ND <br /> Bromochloromethane ND ]sopropylbenzene ND <br /> Bromodicbloromethane ND p4sopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene C hloride" ND <br /> n-Butyl benzene ND Methyi ethyl ketone ' ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'x ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobcnzene ND Styrene' '- ND <br /> Chloroethane ND 1 11,2-Tetrachloroethane ND <br /> I 2-Chloroethyi Vinyl Ether" ND 1 1 2 2-Tetrachloroeth2ne ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1,2,3-Trichloiobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochlorometbane ND I I 1-Ttuhloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoiomethane ND <br /> 1,3-Dichlorobenzene ND 1,23-Trichloropropane ND <br /> [,4-Dichlorobenzene ND 1,2 4-rri methy I benzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trtmethylbenzene ND <br /> ],I-Dichioroethane ND Vinyl Acetate""' _N D <br /> 1,2-Dichloroethane ND Vinyl Chloride"" ND <br /> IJ-Dichloroethene ND Xylenes total "" ND <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2 2-Drchloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Recorenes(%) <br /> cis-1,3-Di chl oropropene ND Dibromotluoromethane 108 <br /> trans-l3-Dichloropropene ND Toluene-d8 103 <br /> Ethylene drbromrde ND 4-Biomolluorobenzene 97 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,w ipes in ug/wipe and all TCLP!SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L vapor samples 0 5 uglL solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (t) 2-butanone, (g) 4-methyl-2- <br /> Pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattem of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> IDHS Cernfcation No 1644 fi Edward Hamilton, Lab Director <br />