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j <br /> 1 <br /> 110 Second Avenue South,#D7, Pacheco,CA 94553-5560 <br /> ' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' btlp//www mgaobell corn E-mail main@mccampbell corn <br /> Date Sampled 05112198 <br /> Advanced GeoEnvironmental Client Project ID Top Filling <br /> 4005 North Wilson Way Date Received 06/17/98 <br /> Stockton,CA 95205 Client Contact Tun Cuellar Date Extracted 06/19-06/20/98 <br /> Ghent P O Date Analyzed 06/19-06/20/98 <br /> .. <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 94578 <br /> Client 1D MW5/6-12-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone` ' ND<10 Ethyibenzene 97 <br /> Benzene 38 Hexachlotabutadsene ND<5 <br /> Bromobenzene ND<5 lodomethane ND<5 <br /> Bromochloromethane ND<5 lsopropy)benzene N D<S <br /> Bromod)chloromethane ND<5 p-Isopropyl toluene ND<5 <br /> I� Bromoform ND<5 Methyl butyl ketone` ' ND<5 <br />`# Bromomethane ND<5 Methylene Chloride"' ND<5 <br /> ti-Butyl benzene ND<5 Methyl ethyl ketone ND<5 <br /> sec-Butyl benzene ND<5 Methyl isobutyl ketone'x ND<5 <br /> tert-Butyl benzene NDS Methyl ten-Butyl Ether(MTBE) -- <br /> Carbon Disulfide ND<5 Napiha)ene NfXS <br /> Carbon Tetrachloride ND<5 n-Propyl benzene ND<5 <br /> Chlorobenzene ND<5 Styrene` ND<5 <br /> Chloroethane NIX5 1,1,1 2-Tetrachloroethane ND<5 <br /> 2-Chloroethyl Vinyl Ether"' ND<5 1 1 2 2-Tetrachloroethane ND<5 <br /> Chloroform ND<5 Tetrachloroethene ND<5 <br />' Chloromethane NDS Toluene" ND<5 <br /> 2-Chlorotoluene NDS ) 2 3-Trtchtombenzene NIRS <br /> 4-Chlarotoluene NDS 1 2 4-Trichlorobenzene ND<5 <br /> D)brornoch)oromcthane ND<5 I 1 I-Tt ichloroethane ND<5 <br /> 1,2-Dibromo-3-chloroptopane ND<5 1 12-Trichloroethane ND<5 <br /> Dibromomethane NDcS Trichloroethene ND<5 <br /> 1,2-Dichlorobenzene ND<5 Tnchlorotluoromethane ND<5 <br /> 1,3-Dichlorobenzene ND<5 1,2,3-Trzchloropropane ND<5 <br /> 1 4-Dichlorobenzene ND<5 1 2,4-Trimetliylbenzene 21 <br /> Dishlorodiiluorornethane NDS I3,5-Trirnethy(benzene ND<5 <br /> I 1-Dichloroethane ND<5 Vinyl Acetate") NDS <br /> 1,2-Dichloroethane ND<5 Vinyl Chloride"' ND<5 <br /> 1 LI-Dichloroethene ND<5 Xylenes Iota! '°' 82 <br /> cis-1 2-Dich)oroethene NIX5 <br /> trans-1 2-Dichloroethene ND<5 <br /> 1,2-Dick loropropane NIX5 <br /> 1,3-Diebloropropane ND<5 <br /> 2,2-Dschloropropane NDcS Comrrttnts <br /> I I-Dichloropropene ND<5 5u rroga to Recoveries('%U) <br /> css-1,3-Drchloropropene ND<5 Dibromotluoromethane 112 <br /> trans-l,3-Dichloropropenc ND<5 Toluene-d8 1103 <br /> Ethylene dibromide ND<5 4-Bromotluorobcnzene 95 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,%ipes in uglwtpe and all TCLP I SPI-P extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L %apor samples 0 5 ug/L solid and sludge samples 5 uglkg, wipes <br /> 0 2ug/wipe ND means not detected above the repotting limit N/A mudris analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-metbyi-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (l)methylbenzene (m)acetic acid ethenyl ester (n)chloroethane (o)dimethylbenzenes <br /> DHS Certification No 1644 Z Edward Hamilton,Lab Director <br />