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I <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ht(y//www mi&gmnbell com E-mail matn@mccampbell com <br /> Advanced GeoEnvironmental Client Project 1D Top Filling Date Sampled 06/I2/98 <br /> 4005 North Wilson Way <br /> Date Received 06/17/98 <br /> Stockton,CA 95205 Client Contact Tun Cuellar Date Extracted 06/19-06/20/98 <br /> Client P O Date Analyzed 06119-06/20/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> I Lab ID 90580 <br /> Client ID VW2/6-12-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> AcetoneN15<7000 Ethylbenzene 3500 <br /> Benzene 44,000 Hexachlorobutadiene ND<3400 <br /> Bromobenzene ND<3400 lodomethane ND<3400 <br /> Bromochloromethane ND<3400 Isopropylbenzene N1K3400 <br /> Bromodichloromethane ND<3400 p4sopropyl toluene ND<3400 <br /> Bromoform ND<3400 Methyl butyl ketone` ND<3400 <br /> Bromomethane ND<3400 Methylene Chloride"' ND<3400 <br /> n-Butyl benzene ND<3400 Methyl ethyl ketone ' ND<3400 <br /> sec-Butyl benzene ND<3400 Methyl isobutyl ketones ND<3400 <br /> tert-Butyl benzene ND<3400 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<3400 Napihalene ND<3400 <br /> Carbon Tetrachloride ND<3400 n-Propyl benzene NDa3400 <br /> Chlombenzene ND<3400 Styrene` ND<3400 <br /> Chloroethane ND<3400 ],I 1 2-Tetrachloroethane ND<3400 <br /> 2-Chloroethyl Vinyl Ethe ND<3400 1,1,2,2-Tetrachloroethane ND<3400 <br /> Chloroform ND<3400 Tetrachloroethene ND<3400 <br /> Chloromethane ND<3400 Toluene" ND<3400 <br /> 2-Chlorotoluene ND<3400 1,2,3-Tnclilorobenzene ND<3400 <br /> 4-Chlorotoluene ND<3400 1,2,4-Tnchlorobenzene ND<3400 <br /> Dibromochloromethane ND<3400 1,1 1-Trichloroethane ND<3400 <br /> 1,2-Dibromo-3-chloropropane ND<3400 1,12-Trichloroethane ND<3400 <br /> Dibromomethane ND<3400 Trichloroethene ND<3400 <br /> I 1,2-Dichlorobenzene ND<3400 Trichlorofluoromethane ND<3400 <br /> 1,3-Dichlorobenzene ND<3400 1,2,3-Trichloropropane ND<3400 <br /> 1,4-Dichlorobenzene ND<3400 1 2,4-Tnmethylbenzene ND<3400 <br /> Dichlorodifluoromethane ND<3400 1,3,5-Trimethylbenzene ND<3400 <br /> I ],1-Dichloroethane ND<3400 Vinyl Acetate""' ND<3400 <br /> 1,2-Dichloroethane ND<3400 Vinyl Chloride"' ND<3400 <br /> I,1-Dichloroethene NIK3400 Xylenes,total '° 15,000 <br /> cis-1,2-Dichlowethene ND<3400 <br /> trans-l,2-Dichloroethene ND<3400 <br /> 1,2-Dichloropropane ND<3400 <br /> 1,3-Dichloropropane ND<3400 <br /> 2,2-Dichloropropane ND<3400 Comments <br /> 1,1-Dichloropropene ND<3400 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<3400 Dibromofluoromethane 102 <br /> trans-1,3-Dichloropropene ND<3400 Toluene-d8 104 <br /> Ethylene dibromide ND<3400 4-Bromofluorobenzene 99 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/uipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, %apor samples 05 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 /_'i Edward Hamilton,Lab Director <br /> E <br />