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l <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 1 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httn//www mg-j-,�com E-mail main@mccampbell com <br /> Date Sampled 06/12/98 <br /> Advanced GeoEnvironmental Client Project ID Top Filling <br /> Date Received 06/17/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Tum Cuellar Date Extracted 06119-06/20/98 <br /> Client P O Date Analyzed 06119-06120198 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 90580 <br /> Client ID VW2/6-12-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<7000 Ethylbenzene 3500 <br /> Benzene 44,000 Hexachlorobuiadienc NIX3400 <br /> Bromobenzene ND<3400 lodomethane ND<3400 <br />' Bromochloromethane ND<3400 Isopropyibenzene ND<3400 <br /> Bromodichloromethane ND<3400 p-Isopropyl toluene NIX3400 <br /> Bromoform ND<3400 Methyl butyl ketoneND<3400 <br /> Brornomethane ND<3400 Methylene Chloride" NLK3400 <br />' n-Butyl benzene ND<3400 Methyl ethyl ketone" ND<3400 <br /> sec-Butyl benzene ND<3400 Methyl isobutyi ketones ND<3400 <br /> tert-Butyl benzene ND<3400 Methyl ten-Butyl Ether(MTBE) -- <br /> Carbon Disulfide ND<3400 Napthalene ND<3400 <br /> Carbon Tetrachloride ND<3400 n-Propyi benzene NLK3400 <br /> Chlorobenzene ND<3400 Styrene` NLK3400 <br /> Chloroethane ND<3400 1,1,1,2-Tetrachl0r0ethane ND<3400 <br /> 2-Chloroethyl Vinyl Ethe ` ND<3400 1,1,2 2-Tetrachloroethane NLK3400 <br /> Chloroform ND<3400 Tetrachloroethene ND<3400 <br /> Chloromethane ND<3400 Toluene" ND<3400 <br /> 2-Chlorotoluene ND<3400 1,2 3-Trichlorobenzene ND<3400 <br /> 4-Chlorotoluene ND<3400 1,2,4-Tnchlorobenzene ND<3400 <br /> Dibromochloroethane ND<3400 1,1 1-Tri chloroethane N D<3400 <br /> m <br /> 1,2-Dibromo-3-chloropropane NLK3400 1,12-Trichloroethane NDX3400 <br /> Dibromomethane ND<3400 Trichloroethene ND<3400 <br /> 1,2-Dichlorobenzene NLK3400 Trichlorofluoromethane ND<3400 <br />' 1,3-Dichlorobenzene ND<3400 1,2 3-Trichloropropane F1DX34(0)0 <br /> FK ('0 <br /> 1,4-Dichlorobenzene ND<3400 1,2 4-Tn methylbenzen a D<3400 <br /> Dichlorodifluoromethane ND<3400 1,3,5-Trimeth}lbenzene ND<3400 <br /> 1,1-Dichloroethane ND<3400 Vinyl Acetate"" D<3400 <br />' 1,2-Dichloroethane NIK3400 Vm}1 Chloride"' <br /> ],1-Dichloroethene ND<3400 X}lenes,total '° 15,000 <br /> cis-1,2-Dichloroethene NLK3400 <br />' trans-] 2-Dichlorocibene ND<3400 <br /> 1,2-Dichloropropane ND<3400 <br /> 1,3-Dichloropropane NL}<3400 <br /> 2,2-Dichloropropane ND<3400 Comments <br /> 1,1-Dichloropropene ND<3400 Surrogate Recoveries("/o) <br /> cis-1,3-Dichloropropene ND<3400 Dibromofluoromethane 102 <br /> trans-1,3-DichloropropeneEl NLK3400 Toluene-d8 144 <br /> Ethylene dibromide ND<3400 4-Bromofluorobenzene 99 <br /> w ater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/,A ipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples ] 0 ug/L, vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (1)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 I—zl Edward Hamilton,Lab Director <br />