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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htttp//www mccampo belI gE-matt main@mccampbell corn <br /> Date Sampled 06/12/98 <br /> Advanced GeoEnvirotnnental Client Project ID Top Filling <br /> Date Received 06/17/98 <br /> 4005 North Wilson Way <br /> Client Contact Tim Cuellar Date Extracted 06/I9-06120198 <br /> Stockton,CA 95205 <br /> [Client P ODate Analyzed 06119-06/20/98 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> 7 <br /> Lab ID 90581 <br /> Client ID VW3/6-12-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ND<4000 Ethylbenzene 3500 <br /> Benzene 36,000 Hexachlorobuladiene ND<2000 <br /> Bromobenzene ND<2000 lodomethane ND<2000 <br /> Bromochloromethane ND<2000 lsopropylbenzene ND<2000 <br /> Bromodichloromethane ND<2000 p-Isopropyl toluene ND<2000 <br /> Bromoform NIX2000 Methyl butyl ketone"" ND<2000 <br /> Bromomethane ND<2000 Methylene Chloride" ND<2000 <br /> n-Butyl benzene ND<2000 Methyl ethyl ketone" ND<2000 <br /> sec-Butyl benzene ND<2000 Methyl isobutyi ketone'y ND<2000 <br /> tert-Butyi benzene ND<2000 Methyl;ten-Butyi Ether(MTBE) <br /> Carbon Disulfide ND<2000 Napthalene ND<2000 <br /> Carbon Tetrachloride ND<2000 n-Propyl benzene ND<2000 <br /> Chlorobenzene ND<2000 Styrene' ' ND<2000 <br /> Chloroethane ND<2000 i,l 12-Tetrachloroethane ND<2000 <br /> 2-Chloroethyl Vmy]Ethe ND<20001,1 2 2-Tetrachloroethane ND<2000 <br /> Chloroform ND<2000 Tetrachloroethene ND<2000 <br /> Chloromethane ND<2000 Toluene"' 43,000 <br /> 2-Chlorotoluene ND<2000 1,2 3 Ti ichlorobenzene ND<2000 <br /> 4-Chlorotoluene ND<2000 1,2,4-Tnchl orobenzene ND<2000 <br />' Dibromochloromethane ND<2000 1,1,1-Trichloroethane ND<2000 <br /> 1 2-Dibromo-3-chloropropane ND<2000 1 1 2 Trichloroethane ND<2000 <br /> Dibromomethane ND<2000 Trichloroethene ND<2000 <br /> 1,2-Dichlorobenzene ND<2000 Trichloiofluoromethane ND<2000 <br />' 1,3 Dichiorobenzene ND<2000 1,2 3-Trichloropropane ND<2000 <br /> 1,4-Dichlorobenzene ND<2000 1 2,4 Trimethylbenzene 2400 <br /> Dichlorodifluoromethane ND<2000 1 1 3 5-TrimethyIbenzene ND<2000 <br /> 1,1-Dichloroethane ND<2000 Vinyl Acetate""' ND<2000 <br /> 1,2-Dichloroethane ND<2000 Vinyl Chloride ND<2000 <br /> 1,1-Dichloroethene ND<2000 Xylenes,total 19,000 <br /> cis-1,2-Dichloroethene ND<2000 <br /> trans-l,2-Dichloroetbene ND<2000 <br /> 1,2-Dichloropropane ND<2000 <br /> 1 3-Dichloropropane ND<2000 <br /> 2,2-Dichloroprop2ne ND<2000 Comments <br /> 1,1-Dichloropropene ND<2000 Surrogate Reew-eries <br />' cis-1,3-Dichloropropene ND<2000 Dibromotluoromethane 107 <br /> trans-] 3-Dichloropropene ND<2000 Toluene-d8 98 <br /> Ethylene dibromide ND<2000 4-Bromoiluorobenzene 99 <br /> water and vapor samples are reported in uglL,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,NIA means anaiyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (1)liquid sample that contains greater than --5 vol % <br /> sediment 0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 /-'L Edward Hamilton,Lab Director <br />