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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 124 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hUP I/www mccatnpbell com E-mail main@mccampbell corn <br /> i <br /> Advanced GeoEnvironmental Client Project ID Top Filling Date Sampled 12/11/01 <br /> 837 Shaw Road Date Received 12/12/01 <br /> Stockton, CA 95215 Client Contact Tian Cuellar Date Extracted 12/20-12/21/01 <br /> Client P Q Date Analyzed 12/20-12/21/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 86153 86I54 86155 86156 <br /> MW5/ MW6A/ MW6B/ MW6C/ Reporting Limit <br /> Client ID 121101 121101 121101 121101 <br /> Matnx W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND<250 ND<5 0 ND 50 t 0 <br /> Ethyl tert-Butyl Ether(FTSE) ND ND<250 ND<5 0 ND 50 1 0 <br /> Methyl tert-Butyl Ether(MTBE) ND 21,000 240 12 50 10 <br /> lie tert-Amyl Methyl Ether(TAME) ND ND<250 ND<5 0 ND so 10 <br /> tert-Butanol ND NIX 1250 ND<25 ND 25 50 <br /> Methanol ND ND<125,000 ND<2500 ND 2500 500 <br /> Ethanol ND ND<12,500 ND<250 ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 110 104 95 111 <br /> Comments <br /> *water samples are reported m ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting lirnit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />