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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAlY1PBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 24 htta//www mccamnbell com E-mail main@mccampbell com <br /> Advanced GeoEnvironmental CIient Project ID Top Filling Date Sampled 12/11/01 <br /> 837 Shaw Road Date Received 12/12/01 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 12/20-12/21/01 <br /> Client P 0 Date Analyzed 12/20-12/21/01 <br /> Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method$264 modified <br /> Lab ID 86157 86158 86159 86160 <br /> Client ID MW6D/ MW6E/ MW7B/ MW7C/ Reporting Limit <br /> 121101 121101 121101 121101 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND ND ND<5 0 ND 50 1 0 <br /> Ethyl tert-Butyi Ether(F-TBE) ND ND ND<5 0 ND 50 10 <br /> Methyl tert-Butyl Ether(MTBE) 1 1 ND 320 ND 50 10 <br /> lie tert-Amyl Methyl Ether(TAME) ND ND ND<5 0 ND 50 1 0 <br /> I <br /> tert-Butanol ND ND ND<25 ND 25 50 <br /> Methanol ND ND ND<2500 ND 2500 500 <br /> Ethanol ND ND ND<250 ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 115 116 84 110 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP I STLC I SPLP extracts to ug/L <br /> ND means not detected above the reporting lirnit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />