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110 2nd Ave.South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 <br /> AJ ht :I/ w.mc a f. m E-mail:main@mccampbell.com <br /> Date Sampled: 02/I8/99 <br /> Castle Analytical Laboratory Client Project ID: ##20621/ 34-99039 <br /> 2333 Shuttle Dr.,Bldg 9081909 Date Received: 02/23/99 <br /> Client Contact: Jim Phillip Date Extracted: 02/23/99 <br /> Atwater, CA 95301 <br /> Client P.O: Date Analyzed: 02/23/99 <br /> Lead* <br /> EPA analytical methods 60101200.7,239.2' <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 03772 S-1 S TTLC ND 102 <br /> 03773 S-2 S TTLC ND 105 <br /> 03774 S-4 S TTLC ND 103 <br /> 03775 S-4 S TTLC ND 102 <br /> 03776 S-6 S TTLC 4.1 101 <br /> 03777 S-7 S TTLC ND 100 <br /> 03778 S-8 S TTLC 5.3 105 <br /> 03779 S-9 S TTLC 6.3 101 <br /> S TTLC 3.0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated;ND means not detected above W TTLC 0.005 mg/L <br /> the reporting limit <br /> STLC,TCLP 0.2 mg/L. <br /> *soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,ar d water samples and all STLC/SPLP/TCLP extracts in mg1L <br /> 'Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br /> samples <br /> 'EPA extraction methods 131 l(TCLP),3010/3020(water,TTLC),3040(orgaiie matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> C surrogate diluted out of range;NIA means surrogate not applicable to this aialysis <br /> &reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than —2 vol. % sediment; this se iment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 ��.� Edward Hamilton,Lab Director <br />