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110 2nd Ave.South,#D7,Pacheco,CA 94553-5560 <br /> WCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> 24 :1/vww.mccampbell.com E-mail:main@mccampbell.com <br /> Date Sampled: 02/18/99 <br /> Castle Analytical Laboratory Client Project 117: #20621/034-99039 <br /> Date Received: 02/23/99 <br /> 2333 Shuttle Dr.,Bldg 9081909 <br /> Client Contact: Jim Phillips Date Extracted: 02123-02124/99 <br /> Atwater, CA 95301 <br /> Client P.O: Date Analyzed: 02/24/99 <br /> Lead* <br /> EPA analytical methods 60101200.7,239.2' <br /> Lab 1D Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 03780 SP-1,2,3,4 Comp S TCLP ND NA <br /> 03781 SP-5,6,7,8 Comp S TCLP ND NA <br /> S TTLC 3.0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated;ND means not detected above W TTLC 0.005 mg/L <br /> the reporting limit <br /> -- STLC,TCLP 0.2 mg/L <br /> "soil and sludge samples are reported its mg/kg,wipe samples in ug/wipe,and water samples and all STLC 1 SPLP/TCLP extracts in mg/L <br /> 'Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br /> samples <br /> EPA extraction methods 1311(TCLP),301013020(water,TTLC),3040(orga is matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> "surrogate diluted out of range;N/A means surrogate not applicable to this analysis <br /> reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than --2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. / <br /> DHS Certification No. 1644 ��f Edward Hamilton,Lab Director <br />