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I 10 Scc£}nd Avenge South,PD7, Pacheco,CA 94553 <br /> M.cCAMPBBLL ANALYTICAL I,NC. Fo1cphone : 510-79S-162() fax :510-798-1622 <br /> UPI/N,vw-mccamkell.com E-mail main@mccampbcll.com <br /> i <br /> i <br /> I <br /> Advanced GeoEnvirottn>;etttal Client Project 1D: 5-Stater Mal ina Date Satnpled: 11/18/97 <br /> Date Received: 11/20/97 <br /> 4005 Notch Wilson Way <br /> Stockton, CA 95205 <br /> Client Contact: Bill Little Date Extracted: 11/20/97 <br /> Client P.O: Date Analyzed: 11120-11124197 <br /> Volatile Organics Tay CIMS <br /> EPA method 8260 <br /> Lab ID 83239 1 <br /> Client ID SP2-3,4 <br /> Matrix S i <br /> Compound Concentration* Compound Concentration* <br /> Acetone Jbi ND<7 Ethylbenzene ND <br /> Benzene ND I-lexachlorobutadi nic ND fl <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluol e ND <br /> Bromoform ND Methyl butyl ketole ND <br /> Bromomethane ND Methylene Chlor/ e" ND <br /> n-Butyl benzene ND Methyl ethyl ketole" ND <br /> sec-Butyl benzene ND Methyl isobutyl k tone's ND <br /> tert-Butyl benzene ND Methyl tort-Butyl Ether(MTBE) --- i <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND StyreneND i <br /> Chloroethane ND 1,1,1,2-Tetrachlo ethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-TetrachInToethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene` ND <br /> 2-Chlorotoluene ND 1,2.3-Trichlorobe zene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobe zene ND <br /> Dibromochloromethane ND 1,1,1-Trichloroet3 ane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroet ane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlor0fluOrOm thane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropr pane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylb irzene ND <br /> Dichloroditluoromethane ND 1,3,5-Trimethylb nzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"" ND <br /> IJ-Dichloroethene ND Xylenes,total '°' ND <br /> cis-1,2-Dichloroethene ND TP H-(g)(C6-Cl ) <br /> trans-1,2-Dichloroethene ND TPH-(ms)(C8-(12) — <br /> 1,2-Dichloropropane ND TP H-(k)(C 10+) <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries(1/6) <br /> cis-1,3-Dichloropropene ND Dibromofluorom thane 107 <br /> trans-1,3-Dichloropropene ND Toiuene-d8 106 <br /> Ethylene dibromide ND 4-Bromotluorobe zene 96 <br /> 'water and vapor samples are reported in ug/t-,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/l.. <br /> Reporting limits unless otherwise stated: water samples 0.5 ug/L; vapor sa i1ples 0.5 ue/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (e) (2-chloroethoxy) ethene: (d) 2-hexanone; (e) dichloromethane; (t) 2-butanone; (g) 4-methyl-2-. <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is pr sent; (i) liquid sample that contains greater than --5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene; o)dimethylbenzenes. <br /> DHS Certification No. 1644 i Edward Hamilton,Lab Director <br />