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I 1 Second Avenue South,ttD7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. " elchhone : 510-798-1620 Fax : 510-798-1622 <br /> httr.11w v«.mccamkt�ell.com E-mail: main a mccampbciLcom <br /> I <br /> Client Project 1D: 5-Starr M,riga Date Sampled: 11/18/97 <br /> Advanced(ieoEnvironnlental l <br /> Date Received: 11/20/97 <br /> 4005 North Wilson Way <br /> I <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 11/20/97 <br /> Client P.O: Date Analyzed: 11/21/97 <br /> Lead* <br /> EPA analytical methods 6010/200.7,239.2' <br /> Lab 1D Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 83234 SPI-1 S TTLC 8.3 99 <br /> 83235 T1-W S TTLC 12 96 <br /> 83236 TI-E S TTLC 9.0 98 <br /> 83237 SP1-2 S TTLC 11 98 <br /> 83238 SP2-1,2 S TTLC 30 98 <br /> 83239 SP2-3,4 S TTLC 23 98 <br /> 83240 SP3-1 S TTLC 19 95 <br /> S TTLC 3.0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated;ND means not detected aboveTTLC 0.005 mg/L <br /> the reporting limit <br /> L-W STLC,TCLP 0.2 mg/L <br /> soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and nater samples and all STLC/SPLP/TCLP extracts in mg/L <br /> }Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br /> samples <br /> °EPA extraction methods [31l(TCLP),301013020(water,TTLC),3040(organk matrices,TTI-C),3050(solids,TTLC);STLC-CA Title 22 <br /> `surrogate diluted out of range;N/A means surrogate not applicable to this ana ysts <br /> 8'reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than --2 voi. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />