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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMTBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http//wwwmccampbellcom E-mail main@mccampbell com <br /> Advanced GeoEnvironmental Client Pro3ect ID Rainwater Car Wash Date Sampled 12/19/00 <br /> ' 4005 North Wilson Way I Date Received 12/20/00 <br /> Stockton, CA 95205 Client Contact Tun Cuellar Date Extracted 12/22-12/28100 <br /> Client P O + Date Analyzed 12/22-12/28/00 <br /> ' Volatile Organics By COMES <br /> EPA method 8260 <br /> Lab ID 56432 <br /> ' – Client ID l SP 85053/ 121900 <br /> Matrix W <br /> Compound Concentration* Repatng L-mit * Reporting Urmt <br /> p W S Compound Concentration <br /> W S <br /> ' Acetone{° ND<10 50 25 trans-1,3-Dtchloropropene ND<10 E5O <br /> 50 <br /> Benzene 22 10 50 Ethylene dibromide ND<10 5 0 <br /> Bromobenzene ND<10 10 5 0 Ethylbenzene ND<10 5 0 <br /> Bromochloromethane ND<10 1 0 50 Hexachlorobutadtene ND<10 25 <br /> ' Brorriodichloromethane ND<10 10 50 lodornethane ND<10 10 5 0 <br /> Bromoform ND<l0 1 0 50 Isopropylbenzene ND<10 10 50 <br /> Bromomethane ND<10 1 0 5 0 p-Isopropyl toluene ND<10 1 0 5 0 <br /> n-Butyl benzene ND<10 1 0 50 Methyl butyl ketone ND<10 l 0 5 0 <br /> ' sec-Butyl benzene _ ND<10 1 0 5 0 Methylene Chloride"' ND<40 —T—o _5_O_ <br /> tert-Butyl benzene ND<10 1 0 5 0 Methyl ethyl ketone ND<10 _i_O__ 10 <br /> Carbon Disulfide ND<10 l 0 50 Methyl isobutyl ketone'81 NI3<10 10 50 <br /> Carbon Tetrachloride LL ND<10 1 0 50 Methyl tert-Butyl Ether(MTBE) — 10 5 0 <br /> Chlorobenzene ND<10 1 0 5 0 Naphthalene ND<10 5 0 5 0 <br /> Chloroethane NEK10 1 0 50 n-Propyl benzene TVD-10 1 0 5 p <br /> 2-Chloroethyl Vinyl Fthcr T NDc10 ] 0 5 0 Styrene ND<10 l 0 5 0 11 <br /> Chloroform --- NiXIO 1 0 50 1,1,1,2-Tetrachloroethane ND<10 10 50 1 <br /> Chloromethane ND<10 10 50 1,1,2,2-Tetrachloroethane I4D<10 10 F502-Chlorotoluene ND<10 1 0 5 0 Tetrachloroethene 200 1 0 4-Chlorotoluene ND<10 1 0 50 Toluene 35 l 0 Mbromochlaromethane ND<10 1 0 5 0 1,2,3-Trichlorvbenzene ND<10 5051,2-Dibromo-3-chloropropane ND<10 2 0 10 1,2,4-Tnchlorobenzene ND<10 0 <br /> Dibromomethane ND<10 1 0 5 0 1,1,1-Tnehloroethane ND<10 10 5 0 <br /> 42-Dichlorobenzene ND<10 10 50 1,1,2-Trichloroethane ND<10 10 50 <br /> ' 1,3-Dichlorobenzene ND<10 t 0 5 0 Trichloroethene 28 1 0 5 0 l <br /> 1,4-13ichlorobenzene ND<10 1 0 5 0 Tnehlorofluoromethane ND<10 _10 —50 <br /> Dichlorodifluoromethane ND<]0 1 0 50 1,2,3-Tnehloropropane ND<10 1-0 5 0 <br /> 1,1-Dichloroethane N13<10 1 0 5 0 1 2,4-Tnmethylbenzene ND<10 1 0 5 0 <br /> 1 2-Dichloroethane ND<10 1 0 50 1,3,5-Trintethylbenzene ND<10 10 5 0 <br /> l,l-Dichloroethene ND<10 l 0 50 Vinyl Acetate m ND<10 5 0 25 <br /> cis-1,2-Dichloreethene 17 1 0 50 Vinyl Chlonde ° ND<10 10 50 <br /> trans-1,2-Dichloroethene ND<]0 1 0 5 0 Xylenes,total 22 10 50 <br /> ' <br /> 1,2-Ihchloropropane ND<10 1 0 5 0 Comments <br /> 1,3-Dichloropropane ND<10 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<10 1 0 5 0 Dibromotluoromethane 103 <br /> 1,1 Dtchloropropene ND<10 1 0 50 Toluene-d8 100 <br /> ' cis-1,3-Dichloropmpene ND<10 1 0 50 4-Bromofluorobenzene 117 <br /> water and vapor samples are reported in ug/1,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPI P extracts in ugrr <br /> ND means not detected above the reporting lirmt N/A means analyte not applicable to this analysis <br /> ' (b) 2-propanone or dimethyl ketone (c)(2-chloroethexy) ethene (d) 2 hexanone, (e)dichloromethane, (t) 2-butanonc (g)4-methyl 2 <br /> pentanone pr isopropylacetone,(h) lighter than water immiscible sheen is present, (1)liquid sample that contains greatei than---5 Nol % <br /> sediment (1) sample diluttd due to high organic Lontent (k) ethenylbenzene, 0) methylbenzene (m) acetic acid ethenyl ester iP) ; <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />