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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> ' McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell corn E-mail main@mccampbell corn <br /> ' Advanced GeoEnvironmental Client Project ID Rainwater Car Wash Date Sampled 12/19/00 <br /> 4005 North Wilson Way Date Received 12/20/00 <br /> tI <br /> Stockton, GA 95205 Client Contact Tiril Cuellar Date Extracted 12/22-12/28100 � <br /> CIient P O Date Analyzed 12/22-12/28/00 <br /> ' <br /> EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 56433 <br /> Client ID SP 883 861 1 21 900 <br /> Matrix W <br /> E <br /> Concentration* Reporting Limit Reporting Limit <br /> ' W SCompound Concentration* W S <br /> ND<13 5 0 25 trans-l,3-Dichloropropene ND<13 10 50 <br /> 17 1 0 5 0 Ethylene dibromide ND<13 1 0 50 <br /> NIX 13 1 0 5 0enzene ND<13 10 50 <br /> romochloromethane ND<13 to 50 Hexachlarobutadiene ND<13 50 25 <br /> Bromodichloromethane ND<13 10 50, lodomethane ND<13 l 0 so <br /> Brornoform ND<13 1-0 5 0 Iso ro Ylbenzene ND<13 l S 0 1 <br /> ' Bromomethane ND<13 10 5 0 p-Isopropyl toluene ND<13 10 5 0 <br /> n-Butyl benzene ND<13 1-0 50 Methyl butyl ketone ND<13 To— 5 0 <br /> sec-Butyl benzene ND<13 __T_() 5 0 Methylene Chloride' ND<50 1 0 50 <br /> tent-Butyl benzeneND<13 1 0 5 0 Methyl ethyl ketone ND<13 20 10 <br /> Carbon Disulfide ND<13 10 5 0 Methyl isobutyl ketone ND<13 1 0 50 <br /> Carbon Tetrachloride ND<13 f 0 50 Methyl tert-Butyl Ether(MTBE) 1 0 50 <br /> Chlorobenzene� _ ND<13 l 0 50 Naphthalene ND-13 5 0 L50 Chloroethane ND<13 1 05 0n-Propyl benzene ND<l3I02-Chloroethyl Vinylther" ND<13 1U S 0 Styrene ND<13 1 0ChloroformND<13I00 ,1,1,2-TetrachioroethaneND<13 1 0Chloromethane _ TNIX13 lD 5 0 1,1,2,2-TetrachloroethaneND<l3 10 <br /> 2-Chlorotoluene ND<13 1 0 S D Tetrachloroethene 120 1 0 50 <br /> ' 4-Chlorotoluene ND<13 1 0 5 0 Toluene – 24 Y 0 S U <br /> Dtbromochlaromethane NI}<13 ] 0 5 0 1,2,3-F2ND<13 50 25 <br /> l 2-Dthromo-3 chloropmpant, ND<13 ___20 10 1,2,4-Trichlorobenzene ND<]3 50 25 <br /> Dtbromomethane NIX13 10 —3-0 1,1,1-Trichloroethane ND<13 1-0 50 <br /> ' 1 2-Dichlorobenzene ND<13 l 0 5 0 1,1,2-Trichloroethane ND<13 1 0 5 0 <br /> 1,3-Dichlorobenzene ND<13 1 0 50 Trichloroethene ND<13 ]0 5 0 <br /> 1,4-Dichlorobenzene NU<13 _F0__—Y-0 Tnchlorofluoromethane ND<13 I O 5 0 <br /> Dichlorodifluoromethane ND<13 10 5 4 1,2,3-Tnchloropropane ND<13 K05 <br /> t,1-Dichlorcethane ND<13 l0 S0 1,2,4-Tnrnethylbe "e ND<13 1,2-Dichloroethane NIX13 1 0 5 0 1,3,5-Trimethylbenzene ND<13 1,1 Dichloroethene ND<13 l0 50 Vinyl AcetateND<13 1,2-Dichloroethene ND<13 10 5 0 Vinyl Chloride " ND�13 trans-l,2-Dicloroethene ND<13 1 0 5 0 Xylcmes,total ND<13 <br /> 1,2-Dichloropropane ND<13 1-0 50 Comments <br /> 1,3-Dichloropropane ND<13 1 0 __5__o Surrogate Recoveries(%} <br /> 2,2-Dichloropropane _ NIX13 1 0 50 Dibromofluoromethane 1 <br /> ' 1,I-Dichlorvpropene ND<13 10 50 Toluene-d8 l0U <br /> cis-I,3-Dtchlvropropene NIX13 ] 0 5 0 4-Bromofluorobenzene 108 <br /> water and vapor samples are reported in ug/l, soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP SPI P extracts in ug/1 <br /> ' ND means not detL ted above the reporting limit N/A means analyte not applicable to this analysis { <br /> (b)2-propanone or dimethyl kctont., (c) (2-Lhlcroethoxy) ethene (d) 2 hexanone, (c) dichioromethane , <br /> io t bu a real (g) 4 MOW <br /> pentanone or tsopropylacetone (h)lighter[hast water immiscible sheen is present, (i)liquid sample that contains greater than--5 vol "„ <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, 1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> ' ehloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director J <br /> 1 <br />