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CLIENT: Pacific Edge Engineering ANALYTICAL QC SUMMARY REPORT <br /> Work Order: N023518 <br /> Project: Manteca Firing Range, 0025 TestCode: 8270SOILSIM_M <br /> Sample ID MB-61657 SampType: MBLK TestCode: 8270SOILSIM Units: pg/Kg Prep Date: 312 212 01 7 Runblo: 114251 <br /> Client ID: PBS Batch ID: 61657 TestNo: EPA 8270CSI EPA 3546 Analysis Date: 312 312 01 7 SegNo: 2600107 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPDLimit Qual <br /> Acenaphthylene ND 5.0 <br /> Anthracene ND 5.0 <br /> Benzo(a)anthracene ND 5.0 <br /> Benzo(a)pyrene ND 5.0 <br /> Benzo(b)8uoranthene ND 5.0 <br /> Benzo(g,h,i)perylene ND 5.0 <br /> Benzo(k)8uoranthene ND 5.0 <br /> Chrysene ND 5.0 <br /> Dibenz(a,h)anthracene ND 5.0 <br /> Fluoranthene ND 5.0 <br /> Fluorene ND 5.0 <br /> Indeno(1,2,3-cd)pyrene ND 5.0 <br /> Naphthalene ND 5.0 <br /> Phenanthrene ND 5.0 <br /> Pyrene ND 5.0 <br /> Surr: 1,2-Dichlorobenzene-d4 25.000 50.00 50.0 20 112 <br /> Surr: 2-Fluorobiphenyl 23.500 50.00 47.0 29 118 <br /> Surr: 4-Terphenyl-dl4 23.500 50.00 47.0 23 136 <br /> Surr: Nitrobenzene-d5 22.000 50.00 44.0 28 122 <br /> Sample ID N023518-008A-MS SampType: MS TestCode: 8270SOILSIM Units: pg/Kg Prep Date: 312 212 01 7 Runblo: 114251 <br /> Client ID: ZZZZZZ Batch ID: 61657 TestNo: EPA 8270CSI EPA 3546 Analysis Date: 312 312 01 7 SegNo: 2600109 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPDLimit Qual <br /> 1-Methylnaphthalene 97.194 5.0 200.4 0 48.5 30 111 <br /> 2-Methylnaphthalene 102.204 5.0 200.4 0 51.0 27 112 <br /> Acenaphthene 99.198 5.0 200.4 0 49.5 23 115 <br /> Acenaphthylene 99.198 5.0 200.4 0 49.5 14 128 <br /> Anthracene 89.679 5.0 200.4 0 44.8 39 107 <br /> Benzo(a)anthracene 107.715 5.0 200.4 0 53.8 28 130 <br /> Qualifiers: <br /> B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded <br /> ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference <br /> O Surrogate Diluted Out Calculations are based on raw values <br /> CAUFORNIAIP:562.219.7435 F.562.219.7436 NEVADAlPJ02.307.2659 FJ02.307.269 <br /> ASSET LABORATORIES 11110 Artesia Blvd.,Ste B,Cerritos,CA 90703 3151 W.Post Rd.,Las Vegas,NV 89118 <br /> ELM Cert 2921 ELM Cert 2676 I NV Cert W00922 <br /> 1e1 Clients vMh Pension end Prolesslonellsms EPA ID CM1638 ORELAP/NELAP Cert 4046 <br /> Page 93 of 99 <br />