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CLIENT: Pacific Edge Engineering ANALYTICAL QC SUMMARY REPORT <br /> Work Order: N023518 <br /> Project: Manteca Firing Range, 0025 TestCode: 8270SOILSIM_M <br /> Sample ID N023518-008A-MS SampType: MS TestCode: 8270SOILSIM Units: pg/Kg Prep Date: 312 212 01 7 Runblo: 114251 <br /> Client ID: ZZZZZZ Batch ID: 61657 TestNo: EPA 8270CSI EPA 3546 Analysis Date: 312 312 01 7 SegNo: 2600109 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPDLimit Qual <br /> Benzo(a)pyrene 94.689 5.0 200.4 0 47.2 28 121 <br /> Benzo(b)8uoranthene 98.196 5.0 200.4 0 49.0 29 146 <br /> Benzo(g,h,i)perylene 107.715 5.0 200.4 0 53.8 26 115 <br /> Benzo(k)8uoranthene 98.196 5.0 200.4 0 49.0 25 148 <br /> Chrysene 90.681 5.0 200.4 0 45.2 18 125 <br /> Dibenz(a,h)anthracene 107.214 5.0 200.4 0 53.5 29 121 <br /> Fluoranthene 95.691 5.0 200.4 0 47.8 21 140 <br /> Fluorene 99.699 5.0 200.4 0 49.8 23 125 <br /> Indeno(1,2,3-cd)pyrene 99.699 5.0 200.4 0 49.8 26 120 <br /> Naphthalene 99.198 5.0 200.4 0 49.5 28 98 <br /> Phenanthrene 91.182 5.0 200.4 0 45.5 17 133 <br /> Pyrene 99.699 5.0 200.4 0 49.8 32 122 <br /> Surr: 1,2-Dichlorobenzene-d4 20.541 50.10 41.0 20 112 <br /> Surr: 2-Fluorobiphenyl 19.539 50.10 39.0 29 118 <br /> Surr: 4-Terphenyl-dl4 17.535 50.10 35.0 23 136 <br /> Surr: Nitrobenzene-d5 18.036 50.10 36.0 28 122 <br /> Sample ID N023518-008A-MSD SampType: MSD TestCode: 8270SOILSIM Units: pg/Kg Prep Date: 312 212 01 7 Runblo: 114251 <br /> Client ID: ZZZZZZ Batch ID: 61657 TestNo: EPA 8270CSI EPA 3546 Analysis Date: 312 312 01 7 SegNo: 2600110 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPDLimit Qual <br /> 1-Methylnaphthalene 123.686 5.0 200.3 0 61.8 30 111 97.19 24.0 20 R <br /> 2-Methylnaphthalene 128.693 5.0 200.3 0 64.2 27 112 102.2 22.9 20 R <br /> Acenaphthene 126.690 5.0 200.3 0 63.3 23 115 99.20 24.3 20 R <br /> Acenaphthylene 126.189 5.0 200.3 0 63.0 14 128 99.20 24.0 20 R <br /> Anthracene 110.165 5.0 200.3 0 55.0 39 107 89.68 20.5 20 R <br /> Benzo(a)anthracene 144.216 5.0 200.3 0 72.0 28 130 107.7 29.0 20 R <br /> Benzo(a)pyrene 127.692 5.0 200.3 0 63.8 28 121 94.69 29.7 20 R <br /> Benzo(b)8uoranthene 127.191 5.0 200.3 0 63.5 29 146 98.20 25.7 20 R <br /> Benzo(g,h,i)perylene 143.215 5.0 200.3 0 71.5 26 115 107.7 28.3 20 R <br /> Qualifiers: <br /> B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded <br /> ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference <br /> O Surrogate Diluted Out Calculations are based on raw values <br /> CAUFORNIAIP:562.219.7435 F.562.219.7436 NEVADAlPJ02.307.2659 FJ02.307.269 <br /> ASSET LABORATORIES 11110 Artesia Blvd.,Ste B,Cerritos,CA 90703 3151 W.Post Rd.,Las Vegas,NV 89118 <br /> ELM Cert 2921 ELM Cert 2676 I NV Cert W00922 <br /> 1e1 Clients vMh Pension end Prolesslonellsms EPA ID CM1638 ORELAP/NELAP Cert 4046 <br /> Page 94 of 99 <br />