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Client Sample Results Client : Antea USA Inc . Job ID : 440-246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : TIE - 15_20190716 Lab Sample ID : 440 =246095 =4 Date Collected : 07/16/19 11 : 08 Matrix : Solid Date Received : 07/18/ 19 07 : 30 Percent Solids : 75 . 2 Method : 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 . 039 0 .0053 mg/Kg �0 07/19/19 11 :23 07/20/19 09 :42 1 Acenaphthylene ND 0.039 0 . 0053 mg/Kg 07/19/19 11 : 23 07/20/19 09 :42 1 Anthracene ND 0 .039 0. 0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Benzo[a]anthracene ND 0 .039 0 .0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Benzo[a]pyrene ND 0 . 039 0 .0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Benzo[b]fluoranthene ND 0 .039 0. 0053 mg/Kg 07/19/19 11 : 23 07/20/19 09 :42 1 Benzo[g , h ,i]perylene ND 0 .039 0.0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Benzo[k]fluoranthene ND 0 . 039 0 .0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Chrysene ND 0 .039 0 . 0053 mg/Kg 07/19/19 11 : 23 07/20/19 09 :42 1 Dibenz(a , h)anthracene ND 0 .039 0. 0053 mg/Kg 1> 07/19/19 11 : 23 07/20/19 09 :42 1 Fluoranthene ND 0 .039 0.0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Fluorene ND 0 . 039 0 .0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Indeno[1 ,2 , 3-cd]pyrene ND 0.039 0. 0053 mg/Kg 07/19/19 11 :23 07/20/19 09 :42 1 Naphthalene ND 0 .039 0. 0053 mg/Kg 07/19/19 11 : 23 07/20/19 09 :42 1 Phenanthrene ND 0 .039 0 .0053 mg/Kg 07/19/19 11 : 23 07/20/19 09 :42 1 Pyrene ND 0 . 039 0 .0053 mg/Kg 3 07/19/19 11 :23 07/20/19 09 :42 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac ! 2-Fluorobiphenyl (Surr) 65 29 - 129 07/19/19 11 :23 0'712011909--42 1 Nitrobenzene-d5 64 29 - 126 07/19/19 11 :23 07/20/19 09:42 1 Terphenyl-d14 78 28 - 145 07/19/19 11 :23 07/20/19 09:42 1 FMethod : 801513/5035 - Gasoline Range Organics ( GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-012) ND 0 .44 0. 17 mg/Kg 07/18/19 09 : 00 07/20/19 15 : 32 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 90 65 - 140 07/18/19 09:06 07/20/19 15:32 1 1FMethod : 8015B - Diesel Range Organics ( DRO ) ( GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C1 3-C22) ND 6 .4 3 .2 mg/Kg 07/19/19 11 : 25 07/20/19 04 :01 1 ORO (C23-C40) 3 . 8 J , DX MB 6.4 3 .2 mg/Kg 07/19/19 11 :25 07/20/19 04 :01 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n-Octacosane 86 40 - 140 07/19/19 11 :25 07/20/19 04:01 1 Method : 60108 - Metals ( ICP ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 5 . 1 2 .6 1 .3 mg/Kg 07/22/1911 :47 07/23/1918 : 35 5 Client Sample ID : T4W = 15_20190716 Lab Sample ID : 440 -246095 -5 Date Collected : 07/16/19 11 : 14 Matrix : Solid Date Received : 07/ 18/19 07 : 30 Percent Solids : 76 . 0 Method : 8260B/5035 - Volatile Organic Compounds (GC/MS ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene ND 0 .0021 0 .0011 mg/Kg 07/18/19 08 : 00 07/20/19 11 :38 1 Ethylbenzene ND 0 .0021 0 .0011 mg/Kg 07/18/19 08 :00 07/20/19 11 :38 1 m , p-Xylene ND 0 .0043 0 . 0021 mg/Kg 3� 07/18/19 08 : 00 07/20/19 11 :38 1 i Methyl-t-Butyl Ether ( MTBE) ND 0 .0053 0 . 0011 mg/Kg 07/18/19 08 : 00 07/20/19 11 : 38 1 Eurofins TestAmerica , Irvine Page 13 of 104 7/25/2019 E