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Client Sample Results Client: Antea USA Inc . Job ID : 440 -246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : T4W= 15_20190716 Lab Sample ID : 440 =246095 -5 Date Collected : 07/ 16/ 19 11 : 14 Matrix : Solid Date Received : 07/ 18/ 19 07 : 30 Percent Solids : 76 . 0 Method : 8260B/5035 - Volatile Organic Compounds (GC/MS ) (Continued ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 0 . 0053 0.0021 mg/Kg 3� 07/18/19 08: 00 07/2011911 : 38 1 o-Xylene ND 0 .0021 0 .0011 mg/Kg 3 07/18/19 08 : 00 07/20/19 11 :38 1 - tert-Butyl alcohol (TBA) NO 0. 11 0 .011 mg/Kg 0711 8/1 9 08: 00 07/20/19 11 :38 1 Toluene ND 0. 0021 0 .0011 mg/Kg 07/18/19 08 :00 07/20/19 11 : 38 1 Xylenes , Total ND 0 .0043 0. 0021 mg/Kg 07/18/19 08 : 00 07/20/19 11 :38 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 94 79 - 120 07/18/19 08:00 07/20/19 11 :38 1 Dibromofluoromethane (Surr) 98 60 - 120 07/18/19 08:00 07/20/19 11 :38 1 Toluene-d8 (Surr) 98 79 - 123 07/18/19 08:00 07/20/19 11 :38 1 Method : 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 .039 0 . 0052 mg/Kg 4� 07/19/1911 :23 07/20/1913 :32 1 Acenaphthylene ND 0 . 039 0. 0052 mg/Kg 3� 07/19/1911 : 23 07/20/1913 :32 1 Anthracene ND 0 .039 0.0052 mg/Kg 07/19/1911 : 23 07/20/1913 : 32 1 Benzo[a]anthracene ND 0 .039 0 . 0052 mg/Kg # 07/19/1911 :23 07/20/1913 : 32 1 Benzo[a]pyrene NO 0 . 039 0. 0052 mg/Kg 07/19/1911 :23 07/20/1913 :32 1 Benzo[b]fluoranthene ND 0.039 0.0052 mg/Kg 07/19/1911 : 23 07/20/1913 : 32 1 Benzo [g , h ,i]perylene ND 0 .039 0 .0052 mg/Kg 07/19/1911 :23 07/20/1913 : 32 1 Benzo[k]fluoranthene ND 0 .039 0. 0052 mg/Kg 07/19/1911 :23 07/20/1913 :32 1 Chrysene ND 0 .039 0. 0052 mg/Kg 07119/1911 : 23 07/20/1913 : 32 1 Dibenz(a , h)anthracene ND 0 .039 0.0052 mg/Kg 07/19/1911 : 23 07/20/1913 : 32 1 Fluoranthene ND 0 .039 0 . 0052 mg/Kg 07/19/1911 :23 07/20/1913 :32 1 Fluorene NO 0 . 039 0 . 0052 mg/Kg 07/1911911 :23 07/20/1913 :32 1 Indeno[1 ,2 , 3-cd] pyrene ND 0.039 0. 0052 mg/Kg 0711 9/1 9 11 : 23 07/20/1913 : 32 1 Naphthalene ND 0 .039 0 .0052 mg/Kg 07/19/1911 : 23 07/20/1913 : 32 1 Phenanthrene ND 0 .039 0 .0052 mg/Kg 07/19/1911 :23 07/20/1913 :32 1 Pyrene NO 0 . 039 0. 0052 mg/Kg 07/19/1911 :23 07/20/1913 :32 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl (Surr) 71 29 - 129 07/19/19 11 :23 07/20/19 13:32 1 Nitrobenzene-d5 70 29 - 126 07/19/19 11 :23 07/20/19 13:32 1 Terphenyl-d14 80 28 - 145 07/19/19 11 :23 07/20/19 13:32 1 Method : 8015B/5035 - Gasoline Range Organics (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-C12) 0 . 17 J , DX 0.43 0. 16 mg/Kg 07/18/19 09 : 00 07/20/19 16 :00 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 121 65 - 140 07/18/19 09:00 07/20/19 16:00 1 Method : 80158 - Diesel Range Organics ( DRO ) (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C1 3-C22) ND 6. 5 3 . 3 mg/Kg 07/19/19 11 :25 07/20/19 04 :22 1 ORO ( C23-C40) 4 . 3 J , DX MB 6 .5 3 .3 mg/Kg 07/19/19 11 :25 07/20/19 04 :22 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac Ln-Octacosane 88 40 -�140 07/19/19 11 :25 07/20/19 04:22 1 Eurofins TestAmerica , Irvine Page 14 of 104 7/25/2019