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Client Sample Results Client : Antea USA Inc . Job ID : 440 -246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : PL1A .Surface_20190716 Lab Sample ID : 440 -246095 -9 Date Collected : 07/ 16/19 11 :48 Matrix : Solid Date Received : 07/ 18/ 19 07 : 30 Percent Solids : 84 . 3 Method : 8260B/5035 - Volatile Organic Compounds (GC /MS ) (Continued ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Toluene ND 0 .0022 0 .0011 mg/Kg 07/18/19 08 :00 07/20/19 18: 10 1 Xylenes , Total ND 0 .0044 0. 0022 mg/Kg 07/18/19 08: 00 07/20/19 18 : 10 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 88 79 - 120 07/18/19 08:00 07/20/19 18: 10 1 Dibromofluoromethane (Surr) 102 60 - 120 07/18/19 08:00 07/20/19 18: 10 1 LToluene-d8 (Surr) 98 79 - 123 07/18/19 08:00 07/20/19 18: 10 1 Method : 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 .035 0 .0047 mg/Kg 07/19/1911 : 23 07/20/1911 : 37 1 Acenaphthylene ND 0 .035 0 .0047 mg/Kg 07/19/1911 : 23 07/20/1911 : 37 1 Anthracene ND 0 . 035 0.0047 mg/Kg 07/19/1911 :23 07/20/1911 : 37 1 Benzo[a]anthracene ND 0 . 035 0. 0047 mg/Kg 07/19/1911 :23 07/20/1911 :37 1 Benzo[a]pyrene ND 0 .035 0. 0047 mg/Kg 07/19/1911 : 23 07/20/1911 :37 1 Benzo[b]fluoranthene ND 0 .035 0 .0047 mg/Kg 07/19/1911 : 23 07/20/1911 : 37 1 Benzo[g , h , i]perylene ND 0 . 035 0 .0047 mg/Kg 07/19/1911 :23 07/20/1911 : 37 1 Benzo [k]fluoranthene ND 0 . 035 0. 0047 mg/Kg 3 07/19/1911 :23 07/20/1911 : 37 1 Chrysene ND 0.035 0. 0047 mg/Kg 3� 07/19/1911 : 23 07/20/1911 :37 1 Dibenz(a , h)anthracene ND 0 .035 0 .0047 mg/Kg 07/19/1911 : 23 07/20/1911 :37 1 Fluoranthene ND 0 .035 0 .0047 mg/Kg 07/19/1911 : 23 07/20/1911 : 37 1 Fluorene ND 0 . 035 0 .0047 mg/Kg 0 07/19/1911 :23 07/20/1911 : 37 1 Indeno[1 , 2 , 3-cd]pyrene ND 0 . 035 0. 0047 mg/Kg 07/19/1911 :23 07/20/1911 : 37 1 Naphthalene 0 . 12 0.035 0. 0047 mg/Kg 07/19/1911 : 23 07/20/1911 :37 1 Phenanthrene ND 0 .035 0 .0047 mg/Kg 07/19/1911 : 23 07/20/1911 :37 1 Pyrene ND 0 .035 0 .0047 mg/Kg 3:� 07/19/1911 :23 07/20/1911 : 37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl (Surr) 74 29 - 129 07/19/19 11 :23 07/20/19 11 :37 1 Nitrobenzene-d5 78 29 - 126 07/19/19 11 :23 07/20/19 11 :37 1 Terphenyl-d14 83 28 - 145 07/19/19 11 :23 07/20/19 11 :37 1 Method : 8015B/5035 - Gasoline Range Organics (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-C12 ) 36 EY 0. 36 0. 14 mg �/Kg 07/18/19 09: 00 07/20/19 20 : 12 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 1062 LH 65 - 140 07/18/19 09:00 07/20/19 20: 12 1 Method : 8015B - Diesel Range Organics ( DRO) (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C13 -C22) 6 . 1 5. 9 2 .9 mg/Kg 07/19/19 11 :25 07/20/19 00 : 34 1 ORO (C23 -C40) 16 MB 5 .9 2 .9 mg/Kg 07/19/19 11 :25 07/20/19 00 : 34 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n-Octacosane 83 40 - 140 07/19/19 11 :25 07/20/19 00:34 1 Method : 6010B - Metals ( ICP ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 7 .9 2 .4 1 .2 mg/Kg 07/22/1911 :47 07/23/1918 : 53 5 Eurofins TestAmerica , Irvine Page 19 of 104 7/25/2019