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Client Sample Results Client: Antea USA Inc . Job ID : 440-246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : PL1B -2_20190716 Lab Sample ID : 440 -246095 - 10 Date Collected : 07/16/19 11 : 50 Matrix : Solid Date Received : 07/18/19 07 : 30 Percent Solids : 92 . 7 Method : 8260B/5035 - Volatile Organic Compounds (GC/MS ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene ND 0 .0015 0. 00073 mg/Kg 07/18/19 08 :00 07/20/19 13 :30 1 Ethylbenzene ND 0 .0015 0 .00073 mg/Kg 07/18/19 08 : 00 07/20/19 13 : 30 1 m , p-Xylene ND 0 . 0029 0.0015 mg/Kg 07/18/19 08: 00 07/20/19 13 : 30 1 Methyl-t-Butyl Ether (MTBE) ND 0 .0037 0.00073 mg/Kg 0 07/18/19 08:00 07/20/19 13 :30 1 Naphthalene ND 0 .0037 0 .0015 mg/Kg 3� 07/18/19 08 :00 07/20/19 13 :30 1 o-Xylene ND 0 . 0015 0 .00073 mg/Kg 07/18/19 08 : 00 07/20/19 13 : 30 1 tert-Butyl alcohol (TBA) ND 0 .073 0.0073 mg/Kg 0 07/18/19 08: 00 07/20/19 13 : 30 1 Toluene ND 0 .0015 0. 00073 mg/Kg 07/18/19 08 : 00 07/20/19 13 :30 1 Xylenes, Total ND 0 .0029 0 .0015 mg/Kg 3x 07/18/19 08 : 00 07/20/19 13 :30 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 79 - 120 07/18/19 08:00 07/20/19 13:30 1 Dibromofluoromethane (Surr) 95 60 - 120 07/18/19 08:00 07/20/19 13:30 1 Toluene-d8 (Surr) 97 79 - 123 07/18/19 08:00 07/20/19 13:30 1 Method : 8270C SIM - Semivolatile Organic Compounds (GC /MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 . 032 0 .0042 mg/Kg 07/19/1911 :23 07/20/1912 :00 1 Acenaphthylene ND 0.032 0 .0042 mg/Kg 07/19/1911 :23 07/20/1912 :00 1 Anthracene ND 0 .032 0.0042 mg/Kg 07/19/1911 : 23 07/20/1912 :00 1 Benzo[a]anthracene ND 0 .032 0. 0042 mg/Kg 0 07/19/1911 : 23 07/20/1912 :00 1 Benzo[a]pyrene ND 0 . 032 0.0042 mg/Kg 07/19/1911 :23 07/20/1912 : 00 1 Benzo[b]fluoranthene ND 0 . 032 0 .0042 mg/Kg 07/19/1911 :23 07/20/1912 :00 1 Benzo[g , h , i]perylene ND 0. 032 0 .0042 mg/Kg 07/19/1911 : 23 07/20/1912 :00 1 Benzo[k]fluoranthene ND 0 .032 0 . 0042 mg/Kg 07/19!1911 : 23 07/20/1912 :00 1 Chrysene ND 0 .032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1912 : 00 1 Dibenz(a , h)anthracene ND 0 .032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1912 : 00 1 Fluoranthene ND 0 . 032 0. 0042 mg/Kg # 07/19/1911 :23 07/20/1912 :00 1 Fluorene ND 0 . 032 0 .0042 mg/Kg 3� 07/19/1911 : 23 07/20/1912 :00 1 Indeno[1 ,2 , 3-cd]pyrene ND 0 .032 0 .0042 mg/Kg 07/19/1911 : 23 07/20/1912 :00 1 Naphthalene 0 .0042 J , DX 0 .032 0. 0042 mg/Kg 07/19/1911 : 23 07/20/1912 :00 1 Phenanthrene ND 0 .032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1912 : 00 1 Pyrene ND 0 .032 0. 0042 mg/Kg 3:� 07/19/1911 :23 07/20/1912 : 00 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl (Surr) 69 29 - 129 07/19/19 11 :23 07/20/19 12:00 1 Nitrobenzene-d5 64 29 - 126 07/19/19 11 :23 07/20/19 12:00 1 Terphenyl-d14 76 28 - 145 07/19/1911 :23 07/20/1912:00 1 Method : 80158/5035 - Gasoline Range Organics ( GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-C12) ND 0. 29 0. 11 mg/Kg 07/18/19 09 : 00 07/23/19 18 :05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 87 65 - 140 07/18/19 09:00 07/23/19 18:05 1 Method : 8015B - Diesel Range Organics ( DRO) (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C13 C22) ND 5 . 3 2 . 7 mg/Kg 07/19/19 11 :25 07/20/19 05 :45 1 ORO ( C23-C40) 2 . 8 J , DX MB 5 . 3 2 .7 mg/Kg 07/19/19 11 : 25 07/20/19 05 :45 1 Eurofins TestAmerica , Irvine Page 20 of 104 7/25/2019 ii