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Client Sample Results Client : Antea USA Inc . Job ID : 440 -246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : PL6 =2_20190716 Lab Sample ID : 440 =246095 - 14 Date Collected : 07/16/ 19 13 : 40 Matrix : Solid Date Received : 07/18/ 19 07 : 30 Method : 82608/5035 - Volatile Organic Compounds (GC/MS ) (Continued ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Naphthalene ND 0 . 0037 0.0015 mg/Kg 07/18/19 08 : 00 07/20/19 12 :25 1 o-Xylene ND 0 . 0015 0 .00074 mg/Kg 07/18/19 08: 00 07/20/19 12 :25 1 tert-Butyl alcohol (TBA) ND 0 . 074 0. 0074 mg/Kg 07/18/19 08:00 07/20/19 12 : 25 1 Toluene ND 0 .0015 0. 00074 mg/Kg 07/18/19 08 :00 07/20/19 12 :25 1 Xylenes , Total ND 0 . 0030 0.0015 mg/Kg 07/18/19 08 : 00 07/20/19 12 :25 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromof1uorobenzene (Surr) 87 79 - 120 07/18/19 08:00 07/20/19 12:25 1 Dibromofluoromethane (Surr) 102 60 - 120 07/18/19 08:00 07/20/19 12:25 1 Toluene-d8 (Surr) 94 79 - 123 07/18/19 08:00 07/20/19 12:25 1 Method : 80156/5035 - Gasoline Range Organics ( GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-C12) ND 0.28 0 . 11 mg/Kg 07/18/19 09 :20 07/22/19 20 :46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 105 65 - 140 07/18/19 09:20 07/22/19 20:46 1 Client Sample ID : DISP1 - PL7 -2_20190716 Lab Sample ID : 440 =246095 - 15 Date Collected : 07/16/19 13 : 48 Matrix : Solid Date Received : 07/ 18/19 07 : 30 Percent Solids : 92 . 3 Method : 826013/5035 - Volatile Organic Compounds (GC/MS ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DiI Fac Benzene ND 0 .0017 0. 00083 mg/Kg 07/18/19 08 :00 07/20/19 14 : 54 1 Ethylbenzene ND 0 . 0017 0. 00083 mg/Kg 07/18/19 08 : 00 07/20/19 14 :54 1 m , p-Xylene ND 0 . 0033 0 .0017 mg/Kg ; 07/18/19 08 : 00 07/20/19 14 :54 1 Methyl-t-Butyl Ether (MTBE) ND 0 . 0042 0 .00083 mg/Kg 07/18/19 08: 00 07/20/19 14 : 54 1 Naphthalene ND 0 . 0042 0. 0017 mg/Kg 07/18/19 08 : 00 07/20/19 14 : 54 1 o-Xylene ND 0 .0017 0 .00083 mg/Kg 07/18/19 08: 00 07/20/19 14: 54 1 tert-Butyl alcohol (TBA) ND 0 .083 0. 0083 mg/Kg 07/18/19 08: 00 07/20/19 14 : 54 1 Toluene ND 0 .0017 0. 00083 mg/Kg 07/18/19 08 : 00 07/20/19 14 :54 1 Xylenes , Total ND 0 . 0033 0 .0017 mg/Kg 07/18/19 08 : 00 07/20/19 14 :54 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 88 79 - 120 07/18/19 08:00 07/20/19 14:54 1 Dibromofluoromethane (Surr) 103 60 - 120 07/18/19 08:00 07/20/19 14:54 1 Toluene-d8 (Surr) 99 79 - 123 07/18/19 08:00 07/20/19 14:54 1 Method : 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 . 032 0.0042 mg/Kg 07/19/1911 :23 07/20/1911 :59 1 Acenaphthylene ND 0 . 032 0 .0042 mg/Kg 07/19/1911 :23 07/20/1911 :59 1 Anthracene ND 0 .032 0 .0042 mg/Kg 07/19/1911 :23 07/20/1911 : 59 1 Benzo[a]anthracene ND 0 .032 0 . 0042 mg/Kg 07/19/1911 : 23 07/20/1911 : 59 1 Benzo [a]pyrene ND 0 .032 0.0042 mg/Kg 07/19/1911 : 23 07/20/1911 : 59 1 Benzo[b]fluoranthene ND 0 .032 0. 0042 mg/Kg 07/19/1911 : 23 07/20/1911 : 59 1 Benzo [g , h ,i]perylene ND 0 .032 0 . 0042 mg/Kg 07/19/1911 : 23 07/20/1911 : 59 1 Benzo[k]fluoranthene ND 0 .032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1911 : 59 1 Chrysene ND 0 .032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1911 :59 1 i Dibenz(a , h) anthracene ND 0 . 032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1911 :59 1 Eurofins TestAmerica , Irvine I i Page 25 of 104 7/25/2019 I 4