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Client Sample Results Client : Antea USA Inc . Job ID : 440-246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : DISP1 - 1PL7 -2_20190716 Lab Sample ID : 440 -246095 - 15 Date Collected : 07/ 16 /19 13 : 48 Matrix : Solid Date Received : 07/18/19 07 : 30 Percent Solids : 92 . 3 Method : 8270C SIM - Semivolatile Organic Compounds ( GC/MS SIM ) ( Continued ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Fluoranthene ND 0 . 032 0 .0042 mg/Kg tc 07/19/1911 : 23 07/20/1911 : 59 1 Fluorene ND 0 .032 0. 0042 mg/Kg 07/19/1911 : 23 07/20/1911 : 59 1 r Indeno[1 ,2 ,3-cd]pyrene ND 0 .032 0.0042 mg/Kg 07/19/1911 :23 07/20/1911 :59 1 Naphthalene ND 0 . 032 0 .0042 mg/Kg 07/19/1911 :23 07/20/1911 : 59 1 Phenanthrene ND 0 .032 0 . 0042 mg/Kg # 07/19/1911 : 23 07/20/1911 : 59 1 Pyrene ND 0 .032 0. 0042 mg/Kg 07/19/1911 :23 07/20/1911 : 59 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl (Surr) 71 29 - 129 07/19/19 11 :23 07/20/19 11 :59 1 Nitrobenzene-d5 68 29 - 126 07/19/19 11 :23 07/20/19 11 :59 1 LTerphenyPd14 77 28 - 145 07/19/19 11 :23 07/20/19 11 :59 1 LMethodo 801513/5035 - Gasoline Range Organics ( GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-C12) ND 0 .28 0. 10 mg/Kg 07/18/19 09 :20 07/22/19 21 : 14 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 95 65 - 140 07/18/19 09:20 07/22/19 21 : 14 1 Method : 80158 - Diesel Range Organics ( DRO ) (GC ) 1 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C13-C22) ND 5 .2 2 .6 mg/Kg 07/19/19 11 :25 07/20/19 06 :48 1 ORO (C23-C40 ) 2 .9 J , DX MB 5 .2 2 .6 mg/Kg 3� 07/19/19 11 :25 07/20/19 06 :48 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac n-Octacosane 86 40 - 140 07/19/19 11 :25 07/20/19 06:48 1 Method : 60108 - Metals (ICP) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Lead 2 .0 J , DX 2 . 1 1 . 1 mg/Kg 0 07/22/1911 :47 07/23/1919 :08 5 Client Sample ID : DISP4B_PL8B -2_20190716 Lab Sample ID : 440 -246095 - 16 Date Collected : 07/ 16/19 14 : 00 Matrix : Solid Date Received : 07/18 /19 07 : 30 Percent Solids : 86 . 0 Method : 826013/5035 - Volatile Organic Compounds (GC/MS ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene ND 0 .0018 0. 00089 mg/Kg 07/18/19 08: 00 07/20/19 15 :22 1 Ethylbenzene ND 0 . 0018 0 .00089 mg/Kg 07/18/19 08 : 00 07/20/19 15 : 22 1 m , p-Xylene ND 0 . 0036 0. 0018 mg/Kg 3� 07/18/19 08 :00 07/20/19 15 :22 1 Methyl-t-Butyl Ether (MTBE) ND 0 . 0045 0 .00089 mg/Kg 07/18/19 08 :00 07/20/19 15 :22 1 Naphthalene ND 0 . 0045 0 .0018 mg/Kg 07/18/19 08 : 00 07/20/19 15 :22 1 o-Xylene ND 0 .0018 0. 00089 mg/Kg 0 07/18/19 08 : 00 07/20/19 15 :22 1 tert-Butyl alcohol (TBA ) 0.011 J , DX ID 0 .089 0 .0089 mg/Kg 07/18/19 08 : 00 07/20/19 15 :22 1 Toluene ND 0 .0018 0. 00089 mg/Kg 3'� 07/18/19 08: 00 07/20/19 15 :22 1 I Xylenes , Total ND 0 .0036 0 . 0018 mg/Kg 07/18/19 08 : 00 07/20/19 15 :22 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 86 79 - 120 07/18/19 08:00 07/20/19 15:22 1 Dibromofluoromethane (Surr) 102 60 - 120 07/18/19 08:00 07/20/19 15:22 1 Toluene-d8 (Surr) 97 79 - 123 07/18/19 08:00 07/20/19 15:22 1 Eurofins TestAmerica , Irvine Page 26 of 104 7/25/2019 I E E