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GeoAnalytical Laboratories, Inc. 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)593-2212 email: info oageoanalyticallab.com Report# F9I2001 Project: Alexander Diesel/Reynoso Diesel Date: 10/03/19 San Joaquin County Environmental Health Date Recd: 09/20/19 1868 East Hazelton Ave Stockton, CA 95205 Inorganic Chemistry- Quality Control GeoAnalytical Laboratories, Inc. Reporting Spike Source %REC RPD Anal to Result Limit Units Level Result %REC Limits RPD Limit Notes Batch F003322-6020-EPA 6020 Prepared: 09/23/19 Analyzed: 09/30/19 Blank(F003322-BLK1) Antimony ND 0.5 mg/kg Arsenic ND 0.5 Barium ND 0.5 " Beryllium ND 0.5 " Cadmium ND 0.5 " Chromium ND 0.5 " Cobalt ND 0.5 " Copper ND 0.5 " Lead ND 1.0 " Nickel ND 0.5 " Selenium ND 0.5 Silver ND 1.0 " Vanadium ND 0.5 " Zinc ND 0.5 " LCS(F003322-BSI) Antimony 3.40 0.5 mg/kg 3.125 109 80-120 Arsenic 6.10 0.5 6.250 98 80-120 Barium 11.2 0.5 12.50 89 80-120 Beryllium 2.83 0.5 3.125 91 80-120 Cadmium 5.95 0.5 6.250 95 80-120 Chromium 11.3 0.5 12.50 90 80-120 Cobalt 11.3 0.5 12.50 90 80-120 Copper 11.4 0.5 12.50 91 80-120 Lead 11.1 1.0 12.50 89 80-120 Nickel 12.1 0.5 12.50 97 80-120 Selenium 5.94 0.5 6.250 95 80-120 Silver 5.39 1.0 6.250 86 80-120 Vanadium 6.30 0.5 6.250 101 80-120 Zinc 13.6 0.5 12.50 109 80-120 LCS Dup(F003322-BSD1) Antimony 3.46 0.5 mg/kg 3.125 111 80-120 2 20 Arsenic 6.13 0.5 6.250 98 80-120 0.4 20 Barium 11.5 0.5 12.50 92 80-120 3 20 Beryllium 2.97 0.5 3.125 95 80-120 5 20 Cadmium 6.16 0.5 6.250 99 80-120 3 20 Chromium 11.3 0.5 12.50 91 80-120 0.3 20 Cobalt 11.4 0.5 12.50 91 80-120 1 20 Copper 11.6 0.5 12.50 92 80-120 2 20 Lead 11.4 1.0 12.50 91 80-120 2 20 Nickel 12.4 0.5 12.50 99 80-120 2 20 Selenium 5.87 0.5 6.250 94 80-120 1 20 Silver 5.63 1.0 6.250 90 80-120 4 20 Certification#2585