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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)593-2212 <br /> email: info@geoanalyticallab.com <br /> Report# F912001 Project: Alexander Diesel/Reynoso Diesel Date: 10/03/19 <br /> San Joaquin County Environmental Health Date Rec'd: 09/20/19 <br /> 1868 East Hazelton Ave <br /> Stockton, CA 95205 <br /> Inorganic Chemistry- Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> Anal to Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch F003322-6020- EPA 6020 Prepared: 09/23/19 Analyzed: 09/30/19 <br /> LCS Dup(F003322-BSD1) <br /> Vanadium 6.21 0.5 mg/kg 6.250 99 80-120 1 20 <br /> Zinc 14.3 0.5 12.50 114 80-120 5 20 <br /> Duplicate(F003322-DUP1) Source: F911819-01 <br /> Antimony 53.6 0.5 mg/kg 50.0 7 20 <br /> Arsenic 560 0.5 520 7 20 <br /> Barium 59.4 0.5 57.4 3 20 <br /> Beryllium ND 0.5 ND 20 <br /> Cadmium 82.7 0.5 82.1 0.8 200 <br /> Chromium 661 0.5 621 6 20 <br /> Cobalt 0.39 0.5 0.34 12 20 <br /> Copper 24.3 0.5 25.6 5 20 <br /> Lead 1720 1.0 1630 5 20 <br /> Nickel 12.5 0.5 12.9 3 20 <br /> Selenium 218 0.5 214 2 20 <br /> Silver 28.6 1.0 18.6 42 20 QR-02 <br /> Vanadium 11.4 0.5 9.82 15 20 <br /> Zinc 647 0.5 604 7 20 <br /> Matrix Spike(F003322-MSI) Source: F911819-01 <br /> Antimony 59.9 0.5 mg/kg 3.125 50.0 318 80-120 QM-07 <br /> Arsenic 588 0.5 6.250 520 NR 80-120 QM-07 <br /> Barium 78.1 0.5 12.50 57.4 166 80-120 QM-07 <br /> Beryllium 4.06 0.5 3.125 ND 130 80-120 QM-07 <br /> Cadmium 97.5 0.5 6.250 82.1 247 80-120 QM-07 <br /> Chromium 676 0.5 12.50 621 440 80-120 QM-07 <br /> Cobalt 12.8 0.5 12,50 0.34 100 80-120 <br /> Copper 40.0 0.5 12.50 25.6 115 80-120 <br /> Lead 1800 1.0 12.50 1630 NR 80-120 QM-07 <br /> Nickel 27.3 0.5 12.50 12.9 116 80-120 <br /> Selenium 241 0.5 6.250 214 431 80-120 QM-07 <br /> Silver 27.1 1.0 6.250 18.6 136 80-120 QM-07 <br /> Vanadium 18.0 0.5 6.250 9.82 131 80-120 QM-07 <br /> Zinc 671 0.5 12.50 604 541 80-120 QM-07 <br /> Certification#2585 <br />