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A6E2186 Eka=-K Lathrop ASSOCIATES BSK Associates Fresno Metals Quality Control Report Spike Source %REC RPD Date Analyte Result RL Units Level Result %REC Limits RPD Limit Analyzed Qual EPA 6020-Quality Control Batch:A607164 Prepared:6/13/2016 Prep Method:EPA 3050B Analyst: MAS Blank Spike Dup(A607164-BSD1) Antimony 100 10 mg/kg 100 105 75-125 1 20 06/14/16 Arsenic 100 2.5 mg/kg 100 101 75-125 5 20 06/14/16 Barium 100 6.2 mg/kg 100 101 75-125 3 20 06/14/16 Beryllium 100 1.2 mg/kg 100 103 75-125 3 20 06/14/16 Cadmium 99 1.2 mg/kg 100 99 75-125 1 20 06/14/16 Chromium 100 12 mg/kg 100 102 75-125 3 20 06/14/16 Cobalt 100 12 mg/kg 100 101 75-125 3 20 06/14/16 Copper 100 5.0 mg/kg 100 100 75-125 2 20 06/14/16 Lead 99 6.2 mg/kg 100 99 75-125 2 20 06/14/16 Molybdenum 100 12 mg/kg 100 101 75-125 5 20 06/14/16 Nickel 100 12 mg/kg 100 100 75-125 5 20 06/14/16 Selenium 110 2.5 mg/kg 100 105 75-125 7 20 06/14/16 Silver 41 12 mg/kg 50 83 75-125 2 20 06/14/16 Thallium 94 2.0 mg/kg 100 94 75-125 1 20 06/14/16 Vanadium 99 12 mg/kg 100 99 75-125 2 20 06/14/16 Zinc 100 62 mg/kg 100 101 75-125 0 20 06/14/16 Matrix Spike(A607164-MSI),Source:A61=0800-01 Antimony 100 10 mg/kg 100 ND 103 75-125 06/14/16 Arsenic 99 2.5 mg/kg 100 ND 99 75-125 06/14/16 Barium 160 6.2 mg/kg 100 52 105 75-125 06/14/16 Beryllium 100 1.2 mg/kg 100 ND 100 75-125 06/14/16 Cadmium 99 1.2 mg/kg 100 ND 99 75-125 06/14/16 Chromium 100 12 mg/kg 100 ND 101 75-125 06/14/16 Cobalt 100 12 mg/kg 100 ND 101 75-125 06/14/16 Copper 100 5.0 mg/kg 100 ND 100 75-125 06/14/16 Lead 97 6.2 mg/kg 100 ND 97 75-125 06/14/16 Molybdenum 98 12 mg/kg 100 ND 98 75-125 06/14/16 Nickel 98 12 mg/kg 100 ND 98 75-125 06/14/16 Selenium 99 2.5 mg/kg 100 ND 99 75-125 06/14/16 Silver 39 12 mg/kg 50 ND 78 75-125 06/14/16 Thallium 91 2.0 mg/kg 100 ND 91 75-125 06/14/16 Vanadium 95 12 mg/kg 100 ND 95 75-125 06/14/16 Zinc 99 62 mg/kg 100 ND 99 75-125 06/14/16 Matrix Spike Dup(A607164-MSD1),Source:A6F0800-01 Antimony 100 10 mg/kg 100 ND 100 75-125 3 20 06/14/16 Arsenic 95 2.5 mg/kg 100 ND 95 75-125 3 20 06/14/16 Barium 150 6.2 mg/kg 100 52 99 75-125 4 20 06/14/16 Beryllium 98 1.2 mg/kg 100 ND 98 75-125 3 20 06/14/16 Cadmium 96 1.2 mg/kg 100 ND 96 75-125 4 20 06/14/16 Chromium 91 12 mg/kg 100 ND 91 75-125 10 20 06/14/16 Cobalt 95 12 mg/kg 100 ND 95 75-125 6 20 06/14/16 Copper 94 5.0 mg/kg 100 ND 94 75-125 6 20 06/14/16 Lead 95 6.2 mg/kg 100 ND 95 75-125 2 20 06/14/16 Molybdenum 94 12 mg/kg 100 ND 94 75-125 5 20 06/14/16 A6E2186 FINAL 06272016 1817 Printed:6/27/2016 ***Amended Report **" Page 26 of 33 QA-RP-0001-10 Final.rpt www.BSKAssociates.com