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A6E2186 E3="n-K Lathrop ASSOCIATES BSK Associates Fresno Metals Quality Control Report Spike Source %REC RPD Date Analyte Result RL Units Level Result %REC Limits RPD Limit Analyzed Qual EPA 6020-Quality Control Batch:A607164 Prepared:6/13/2016 Prep Method:EPA 3050B Analyst: MAS Matrix Spike Dup(A607164-MSD1),Source:A61=0800-01 Nickel 92 12 mg/kg 100 ND 92 75-125 6 20 06/14/16 Selenium 96 2.5 mg/kg 100 ND 96 75-125 3 20 06/14/16 Silver 38 12 mg/kg 50 ND 76 75-125 3 20 06/14/16 Thallium 91 2.0 mg/kg 100 ND 91 75-125 0 20 06/14/16 Vanadium 91 12 mg/kg 100 ND 91 75-125 4 20 06/14/16 Zinc 95 62 mg/kg 100 ND 95 75-125 4 20 06/14/16 EPA 6020A-Quality Control Batch:A606481 Prepared:5/31/2016 Prep Method:EPA 3010A for STLC/DISTLC Analyst: MAS Blank(A606481-BLK1) Mercury,WET ND 0.020 mg/L 06/01/16 Blank Spike(A606481-BS1) Mercury,WET 0.19 0.020 mg/L 0.20 97 75-125 06/01/16 Blank Spike Dup(A606481-BSD1) Mercury,WET 0.19 0.020 mg/L 0.20 96 75-125 1 20 06/01/16 Duplicate(A606481-DUPI),Source:A6E2201-01 Mercury,WET ND 0.020 mg/L ND 20 06/01/16 Matrix Spike(A606481-MSI),Source:A6E2201-01 Mercury,WET 0.20 0.020 mg/L 0.20 ND 98 75-125 06/01/16 Matrix Spike(A606481-MS2),Source:A6E2186-06 Mercury,WET 0.19 0.020 mg/L 0.20 ND 97 75-125 06/01/16 Matrix Spike Dup(A606481-MSD1),Source:A6E2201-01 Mercury,WET 0.19 0.020 mg/L 0.20 ND 94 75-125 4 20 06/01/16 Matrix Spike Dup(A606481-MSD2),Source:A6E2186-06 Mercury,WET 0.20 0.020 mg/L 0.20 ND 100 75-125 3 20 06/01/16 EPA 6020A-Quality Control Batch:A606620 Prepared:6/2/2016 Prep Method: EPA 3010A for TCLP Analyst: MAS Blank(A606620-BLKI) Mercury,TCLP ND 0.020 mg/L 06/02/16 Blank Spike(A606620-BS1) Mercury,TCLP 0.20 0.020 mg/L 0.20 99 75-125 06/02/16 Blank Spike Dup(A606620-BSD1) A6E2186 FINAL 06272016 1817 Printed:6/27/2016 `"*Amended Report *' QA-RP-0001-10 Final.rpt www.BSKAssociates.com Page 27 of 33