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819 Striker Avenue,Suite 8 <br /> Sequoia Sacramento,CA 95834. <br /> (916)921-9600 <br /> FAXAnal is .�6}921 � <br /> EMCON/IT-Sacramento Project: Corral Hollow Landfill,San Joaquin County <br /> 1326 N.Market Blvd. Project Number: 791291 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 10/03/01 17:07 <br /> Volatile Organic Compounds by EPA Method 8260B -Quality Control <br /> Sequoia Analytical -Sacramento <br /> Reporting Spike Source oiREC RPD <br /> Result MDL Limit Units Level Result °/"REC Limits RPD Limit Notes <br /> Batch 1100016-EPA 5030B [P/TJ <br /> Blank(1100016-BLKI) Prepared&Analyzed: 10/02/01 <br /> p-Isopropyltoluene ND 0.31 2.0 ug/l <br /> Methylene chloride 2.15 2.1 5.0 J <br /> Methyl cert-butyl ether ND 0.57 2.0 " <br /> Naphthalene 1.10 0.61 5.0 J <br /> n-Propylbenzene ND 0.29 2.0 " <br /> Styrene ND 0.20 2.0 " <br /> 1,1,1,2-Tetrachloroethane ND 0.17 2.0 " <br /> 1,1,2,2-Tetrachloroethane ND 0.50 2.0 " <br /> Tetrachloroethene ND 0.27 2.0 " <br /> Toluene ND 0.27 2.0 " <br /> 1.2,3-Trichlorobenzcne ND 0.41 2.0 " <br /> 1,2,4-Trichlorobenzene ND 0.49 2.0 " <br /> 1,1,1-Trichloroethane ND 0.27 2.0 " <br /> 1,1,2-Trichloroethane ND 0.29 2.0 " <br /> Trichloroethene ND 0.38 2.0 " <br /> Trichlorofluoromethane ND 0.36 5.0 " <br /> 1,2,3-Trichloropropane ND 0.53 2.0 " <br /> 1,2,4-Trimethylbenzene ND 0.31 2.0 " <br /> 1,3,5-Trimethylbenzene ND 0.32 2.0 " <br /> Vinyl chloride ND 0.66 2.0 " <br /> Total Xylenes ND 0.56 2.0 " <br /> Surrogate:Dibromofluoromethane 48.5 50.0 97.0 70-130 <br /> Surrogate:1,2-DCA-d4 52.1 50.0 104 70-130 <br /> Surrogate:Toluene-d8 53.7 50.0 107 70-130 <br /> Surrogate:4-BFB 49.5 50.0 99.0 70-130 <br /> c <br /> LCS(1100016-BS1) Prepared&Analyzed: 10/02/01 <br /> Benzene 54.8 0.33 2.0 ugtI 50.0 tt ` 110 70-130 <br /> Chlorobenzene 52.1 0.26 2.0 50.0 104 70-130 <br /> 1,1-Dichloroethene 56.6 0.61 2.0 50.0 113 70-130 <br /> Toluene 52.7 0.27 2.0 50.0 105 70-130 <br /> Trichloroethene 56.4 0.38 2.0 50.0 113 70-130 <br /> Surrogate:Dibromofluoromethane 49.6 50.0 99.2 70-130 <br /> Surrogate:1,2-DCA-d4 53.0 50.0 106 70-130 <br /> Surrogate:Toluene-d8 53.1 50.0 106 70-130. <br /> Surrogate:4-BFB 46.3 50.0 91.6 70-130 <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Page 4 of 6 <br />