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. ® 819 Striker Avenue.Suite 8 <br /> crdSequoia � t(916)9 1-9600 <br /> IDFAX(916)921-0100 <br /> Analvtical "-seqUOIalabsCOm <br /> EMCON/IT-Sacramento Project: Corral Hollow Landfill,San Joaquin County <br /> 1326 N.Market Blvd. Project Number: 791291 Reported: <br /> Sacramento CA,95834 Project Manager: Steve Giacomini 10,03/01 17:07 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result MDL Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 1100016-EPA 5030B[P/T] <br /> Matrix Spike(1100016 MSI) Source,•5109280-03 Prepared&Analyzed: 10/02/01 <br /> Benzene 53.3 0.33 2.0 ug/l 50.0 ND 107 60-140 <br /> Chlorobenzene 52.4 0.26 2.0 50.0 ND 105 60-140 <br /> 1,1-Dichloroethene 51.5 0.61 2.0 50.0 ND 103 60-140 <br /> Toluene 53.6 0.27 2.0 50.0 0.31 107 60-140 <br /> Trichloroethene 55.1 0.38 2.0 50.0 ND 110 60-140 <br /> Surrogate:Dibromofluoromethane 47.4 50.0 94.8 70-130 <br /> Surrogate:1,2-DCA-d4 48.8 JM 97.6 70-130 <br /> Surrogate:Toluene-d8 54.0 50.0 108 70-130 <br /> Surrogate:4-BFB 46.9 50.0 93.8 70-130 <br /> Matrix Spike Dup(1100016-`ISDI) Source:S109280-03 Prepared&Analyzed: 10/02/01 <br /> Benzene 53.5 0.33 2.0 ug/l 50.0 ND 107 60-140 0.375 25 <br /> Chlorobenzene 52.4 0.26 2.0 50.0 ND 105 60-140 0.00 ' <br /> 1,l-Dichloroethene 53.8 0.61 2.0 " 50.0 ND 108 60-140 4.37 25 <br /> Toluene 53.5 0.27 2.0 50.0 0.31 106 60-140 0.187 25 <br /> Trichloroethene 54.7 0.38 2.0 50.0 ND 109 60-140 0.729 25 <br /> Surrogate:Dibromofluoromethane 49.5 50.0 99.0 70-130 <br /> Surrogate: 1,2-DCA-d4 52.7 50.0 105 70-130 <br /> Surrogate:Toluene-& 53.9 50.0 108 70-130 <br /> Surrogate:4-BFB 49.3 50.0 98.6 70-130 <br /> ee <br /> �r <br /> ,tf <br /> Sequoia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chair of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Page 5 of 6 <br />