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Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3 Job Number: C41950 Account: DECASM Dysert Environmental Project: Pactiv Packaging-4545 Qantas Lane Stockton CA 95206 Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch C41974-IMS L44731.D 1 09/28/15 XB n/a n/a VL1343 C41974-IMSD L44732.1) 1 09/28/15 XB n/a n/a VL1343 U' C41974-1 L44725.D 1 09/28/15 XB n/a n/a VL1343 s The QC reported here applies to the following samples: Method: SW846 8260B C41950-1 C41974-1 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 67-64-1 Acetone ND 150 144 96 148 139 94 4 59-143/27 71-43-2 Benzene ND 37.5 30.3 81 37 29.5 80 3 80-122/13 108-86-1 Bromobenzene ND 37.5 30.5 81 37 28.6 77 6 76-122/12 74-97-5 Bromochloromethane ND 37.5 31.3 84 37 30.1 81 4 81-126/13 75-27-4 Bromodichloromethane ND 37.5 32.6 87 37 31.0 84 5 76-124/13 75-25-2 Bromoform ND 37.5 35.0 93 37 33.5 91 4 72-134/14 104-51-8 n-Butylbenzene ND 37.5 26.4 70* 37 23.7 64* 11 76-122/14 135-98-8 sec-Butylbenzene ND 37.5 27.9 74* 37 25.7 70* 8 77-124/14 98-06-6 tert-Butylbenzene ND 37.5 31.1 83 37 29.2 79 6 76-124/13 108-90-7 Chlorobenzene ND 37.5 30.5 81 37 28.9 78 5 78-122/12 75-00-3 Chloroethane ND 37.5 27.6 74 37 26.2 71 5 71-126/16 67-66-3 Chloroform ND 37.5 29.6 79 37 28.5 77* 4 79-126/13 95-49-8 o-Chlorotoluene ND 37.5 28.9 77 37 26.8 72* 8 73-124/15 106-43-4 p-Chlorotoluene ND 37.5 27.4 73 37 25.4 69* 8 73-127/16 56-23-5 Carbon tetrachloride ND 37.5 33.7 90 37 32.7 88 3 78-127/15 75-34-3 1,1-Dichloroethane ND 37.5 28.0 75* 37 27.0 73* 4 76-123/14 75-35-4 1,1-Dichloroethylene ND 37.5 28.1 75 37 27.6 75 2 73-124/15 563-58-6 1,1-Dichloropropene ND 37.5 31.2 83 37 30.3 82 3 78-126/14 96-12-8 1,2-Dibromo-3-chloropropane ND 37.5 31.3 84 37 29.3 79 7 62-127/21 106-93-4 1,2-Dibromoethane ND 37.5 32.6 87 37 30.8 83 6 76-123/13 107-06-2 1,2-Dichloroethane ND 37.5 32.4 87 37 31.4 85 3 74-125/12 78-87-5 1,2-Dichloropropane ND 37.5 29.1 78 37 27.7 75* 5 76-123/12 142-28-9 1,3-Dichloropropane ND 37.5 30.9 83 37 29.0 78 6 77-121/13 108-20-3 Di-Isopropyl ether ND 37.5 26.3 70* 37 25.4 69* 3 71-126/14 594-20-7 2,2-Dichloropropane ND 37.5 29.5 79 37 27.9 75* 6 77-132/17 124-48-1 Dibromochloromethane ND 37.5 33.6 90 37 32.0 87 5 73-127/13 75-71-8 Dichlorodifluoromethane ND 37.5 44.2 118 37 41.7 113 6 52-141/20 156-59-2 cis-1,2-Dichloroethylene ND 37.5 29.2 78* 37 28.3 77* 3 80-124/13 10061-01-5 cis-1,3-Dichloropropene ND 37.5 30.4 81 37 29.7 80 2 77-125/13 541-73-1 m-Dichlorobenzene ND 37.5 28.5 76 37 26.2 71* 8 76-123/12 95-50-1 o-Dichlorobenzene ND 37.5 28.9 77 37 26.8 72* 8 76-123/12 106-46-7 p-Dichlorobenzene ND 37.5 28.2 75* 37 25.9 70* 9 77-121/12 156-60-5 trans-1,2-Dichloroethylene ND 37.5 30.1 80 37 28.7 78 5 78-123/15 10061-02-6 trans-1,3-Dichloropropene ND 37.5 32.3 86 37 30.3 82 6 71-122/13 100-41-4 Ethylbenzene ND 37.5 30.8 82 37 29.2 79 5 79-121/13 637-92-3 Ethyl tert-Butyl Ether ND 37.5 28.5 76 37 27.5 74* 4 76-131/13 * = Outside of Control Limits. 24 of 40 E ACCIJTEST. C41950